Pyrrolidine, 1-[3-(butylthio)-1-thioxopropyl]- (9CI)

Base Information

Chemical Name:Pyrrolidine, 1-[3-(butylthio)-1-thioxopropyl]- (9CI)
CAS No.:73199-97-0
Molecular Formula:C₁₁H₂₁NS₂
Molecular Weight:231.426
Hs Code.:
Mol file:73199-97-0.mol

Synonyms:Pyrrolidine,1-[3-(butylthio)-1-thioxopropyl]- (9CI)

Suppliers and Price of Pyrrolidine, 1-[3-(butylthio)-1-thioxopropyl]- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of Pyrrolidine, 1-[3-(butylthio)-1-thioxopropyl]- (9CI)

Chemical Property:

PSA：60.63000
LogP:3.27090

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Pyrrolidine, 1-[3-(butylthio)-1-thioxopropyl]- (9CI)

There total 2 articles about Pyrrolidine, 1-[3-(butylthio)-1-thioxopropyl]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 73199-87-8
1-<3-(Butylthio)propanoyl>azacyclopentane

: 73199-97-0
1-<3-(Butylthio)propanethioyl>azacyclopentane

Guidance literature:: With diphosphorus pentasulfide; In xylene; for 1h; Heating;
DOI:10.1021/jo01298a022

Reference yield:

: 22002-73-9
3-(butylthio)propionic acid

: 73199-97-0
1-<3-(Butylthio)propanethioyl>azacyclopentane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) thionyl chloride, dimethylformamide / 1.) room temperature, 16 h, 2.) dichloromethane, added over 30 min to ice-cold solution, then room temperature, 1 h

2: 63 percent / phosphorus pentasulfide / xylene / 1 h / Heating

With diphosphorus pentasulfide; thionyl chloride; N,N-dimethyl-formamide; In xylene;
DOI:10.1021/jo01298a022