N'-perfluorocyclohexancarbonyl-perfluorocyclohexancarbohydrazide

Base Information

• Chemical Name: N'-perfluorocyclohexancarbonyl-perfluorocyclohexancarbohydrazide
• CAS No.: 33843-76-4
• Molecular Formula: C₁₄H₂F₂₂N₂O₂
• Molecular Weight: 648.147
• Mol file: 33843-76-4.mol

Synonyms:N'-perfluorocyclohexancarbonyl-perfluorocyclohexancarbohydrazide

Chemical Property of N'-perfluorocyclohexancarbonyl-perfluorocyclohexancarbohydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N'-perfluorocyclohexancarbonyl-perfluorocyclohexancarbohydrazide

There total 3 articles about N'-perfluorocyclohexancarbonyl-perfluorocyclohexancarbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1,2,2,3,3,4,4,5,5,6,6-undecafluorocyclohexanecarbonyl chloride (58816-79-8) + perfluorocyclohexancarbohydrazide (33843-80-0) → N'-perfluorocyclohexancarbonyl-perfluorocyclohexancarbohydrazide (33843-76-4)

Guidance literature:

In diethyl ether; addn. of soln. of C6F11C(O)NHNH2 in ether to C6F11C(O)Cl, shaking, standing 1 h, then heating by reflux (3-4 h);

Reference yield:

perfluorocyclohexancarbohydrazide (33843-80-0) → N'-perfluorocyclohexancarbonyl-perfluorocyclohexancarbohydrazide (33843-76-4)

Guidance literature:

With acetyl chloride; In diethyl ether;

Reference yield:

cyclo-C6F11C(O)OCH3 (307-13-1) → N'-perfluorocyclohexancarbonyl-perfluorocyclohexancarbohydrazide (33843-76-4)

Guidance literature:

Multi-step reaction with 2 steps

1: N₂H₄*H₂O / methanol

2: AcCl / diethyl ether

With hydrazine hydrate; acetyl chloride; In methanol; diethyl ether;

upstream raw materials:

perfluorocyclohexancarbohydrazide

cyclo-C₆F₁₁C(O)OCH₃

1,2,2,3,3,4,4,5,5,6,6-undecafluorocyclohexanecarbonyl chloride

Downstream raw materials:

2,5-bis-undecafluorocyclohexyl-[1,3,4]oxadiazole