2,5-bis(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-1,4-diketo-3,6-bis(4-ethynylphenyl)pyrrolo[3,4-c]pyrrole

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Chemical Name:2,5-bis(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-1,4-diketo-3,6-bis(4-ethynylphenyl)pyrrolo[3,4-c]pyrrole
CAS No.:1454901-99-5
Molecular Formula:C₃₆H₄₀N₂O₈
Molecular Weight:628.722
Hs Code.:

Synonyms:2,5-bis(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-1,4-diketo-3,6-bis(4-ethynylphenyl)pyrrolo[3,4-c]pyrrole

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Chemical Property of 2,5-bis(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-1,4-diketo-3,6-bis(4-ethynylphenyl)pyrrolo[3,4-c]pyrrole

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Technology Process of 2,5-bis(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-1,4-diketo-3,6-bis(4-ethynylphenyl)pyrrolo[3,4-c]pyrrole

There total 4 articles about 2,5-bis(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-1,4-diketo-3,6-bis(4-ethynylphenyl)pyrrolo[3,4-c]pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1454901-98-4
2,5-bis(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-1,4-diketo-3,6-bis(4-((triisopropylsilyl)ethynyl)phenyl)pyrrolo[3,4-c]pyrrole

: 1454901-99-5
2,5-bis(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-1,4-diketo-3,6-bis(4-ethynylphenyl)pyrrolo[3,4-c]pyrrole

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c3cc44728f

Reference yield:

: 52995-76-3
1-chloro-3,6,9-trioxadecane

: 1454901-99-5
2,5-bis(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-1,4-diketo-3,6-bis(4-ethynylphenyl)pyrrolo[3,4-c]pyrrole

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate / N,N-dimethyl-formamide / 16 h / 120 °C / Inert atmosphere

2: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / tetrahydrofuran / 16 h / 65 °C / Schlenk technique; Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; 2: |Sonogashira Cross-Coupling;
DOI:10.1039/c3cc44728f

Reference yield:

: 84632-54-2
3,6-bis(4-bromophenyl)-2,5-dihydropyrrolo[3, 4-c]pyrrole-1,4-dione

: 1454901-99-5
2,5-bis(2-(2-(2-methoxyethoxy)ethoxy)ethyl)-1,4-diketo-3,6-bis(4-ethynylphenyl)pyrrolo[3,4-c]pyrrole

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate / N,N-dimethyl-formamide / 16 h / 120 °C / Inert atmosphere

2: triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / tetrahydrofuran / 16 h / 65 °C / Schlenk technique; Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide; 2: |Sonogashira Cross-Coupling;
DOI:10.1039/c3cc44728f