Technology Process of C17H18O5
There total 8 articles about C17H18O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
AD-mix-β; water;
In
tert-butyl alcohol;
at 25 ℃;
for 8h;
optical yield given as %ee;
enantioselective reaction;
Inert atmosphere;
DOI:10.1002/anie.200900264
- Guidance literature:
-
Multi-step reaction with 7 steps
1: Inert atmosphere
2: n-butyllithium / Inert atmosphere
3: hydrogenchloride / ethanol; water / Inert atmosphere
4: acetic acid / Inert atmosphere
5: potassium carbonate / Inert atmosphere
6: potassium tert-butylate / Inert atmosphere
7: AD-mix-β; water / Inert atmosphere
With
hydrogenchloride; n-butyllithium; AD-mix-β; potassium tert-butylate; water; potassium carbonate; acetic acid;
In
ethanol; water;
4: Duff reaction / 7: Sharpless dihydroxylation;
DOI:10.1016/j.tet.2011.04.094
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogenchloride / ethanol; water / Inert atmosphere
2: acetic acid / Inert atmosphere
3: potassium carbonate / Inert atmosphere
4: potassium tert-butylate / Inert atmosphere
5: AD-mix-β; water / Inert atmosphere
With
hydrogenchloride; AD-mix-β; potassium tert-butylate; water; potassium carbonate; acetic acid;
In
ethanol; water;
2: Duff reaction / 5: Sharpless dihydroxylation;
DOI:10.1016/j.tet.2011.04.094