3-(9-Anthryl)-2'-hydroxyacrylophenone

Base Information

Chemical Name:3-(9-Anthryl)-2'-hydroxyacrylophenone
CAS No.:36715-65-8
Molecular Formula:C₂₃H₁₆O₂
Molecular Weight:324.379
Hs Code.:
European Community (EC) Number:653-396-8
Nikkaji Number:J3.040.798I
Wikidata:Q76312228

Synonyms:AKOS024334150;3-(9-ANTHRYL)-2'-HYDROXYACRYLOPHENONE;3-(9-Anthryl)-1-(2-hydroxyphenyl)-2-propene-1-one

Suppliers and Price of 3-(9-Anthryl)-2'-hydroxyacrylophenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
3-(9-ANTHRYL)-2'-HYDROXYACRYLOPHENONE AldrichCPR
250mg
$ 144.00

American Custom Chemicals Corporation
3-(9-ANTHRYL)-2'-HYDROXYACRYLOPHENONE 95.00%
5MG
$ 499.65

Total 1 raw suppliers

Chemical Property of 3-(9-Anthryl)-2'-hydroxyacrylophenone

Chemical Property:

XLogP3:6.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:324.115029749
Heavy Atom Count:25
Complexity:474

Purity/Quality:

98%,99%, ^*data from raw suppliers

3-(9-ANTHRYL)-2'-HYDROXYACRYLOPHENONE AldrichCPR ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=C3C=CC=CC3=C2C=CC(=O)C4=CC=CC=C4O
Isomeric SMILES:C1=CC=C2C(=C1)C=C3C=CC=CC3=C2/C=C/C(=O)C4=CC=CC=C4O

Technology Process of 3-(9-Anthryl)-2'-hydroxyacrylophenone

There total 4 articles about 3-(9-Anthryl)-2'-hydroxyacrylophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 118-93-4,104809-67-8
o-hydroxyacetophenone

: 642-31-9
9-anthracene aldehyde

: 36715-65-8
1-(2-hydroxyphenyl)-3-anthracen-9-ylprop-2-en-1-one

Guidance literature:: With barium hydroxide octahydrate; In ethanol; at 60 - 80 ℃;
DOI:10.1002/ejoc.201200838

Reference yield: 33.0%

: 118-93-4,104809-67-8
o-hydroxyacetophenone

: 642-31-9
9-anthracene aldehyde

: 36715-65-8
(E)-3-(anthracen-9-yl)-1-(2-hydroxyphenyl)prop-2-en-3-one

Guidance literature:: With sodium hydroxide; In ethanol; at 20 ℃; for 20h;
DOI:10.1016/j.tetlet.2021.153480

Reference yield:

: 120-12-7
anthracene

: 36715-65-8
(E)-3-(anthracen-9-yl)-1-(2-hydroxyphenyl)prop-2-en-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: POCl₃ / 80 °C

2: ethyl acetate; HCl / 2-taegiges Stehenlassen der Reaktionsloesung

With hydrogenchloride; ethyl acetate; trichlorophosphate;
DOI:10.1021/ja01257a027