Technology Process of C24H33IN2O3
There total 7 articles about C24H33IN2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Iodine monochloride; calcium carbonate;
In
methanol; water;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 1.5 h
2.1: hydrogenchloride; hydrogen / palladium on activated charcoal / methanol; water / 1.5 h / 20 °C
3.1: toluene-4-sulfonic acid / 1,4-dioxane / 22 h / 100 °C / Reflux
3.2: Saturated solution
4.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C / Inert atmosphere
4.2: 0.17 h / 20 °C
5.1: Iodine monochloride; calcium carbonate / methanol; water / 20 °C
With
hydrogenchloride; hydrogen; Iodine monochloride; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; calcium carbonate; potassium iodide;
palladium on activated charcoal;
In
1,4-dioxane; methanol; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sulfuric acid; water; sodium nitrite / 0 - 5 °C
2.1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 1.5 h
3.1: hydrogenchloride; hydrogen / palladium on activated charcoal / methanol; water / 1.5 h / 20 °C
4.1: toluene-4-sulfonic acid / 1,4-dioxane / 22 h / 100 °C / Reflux
4.2: Saturated solution
5.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C / Inert atmosphere
5.2: 0.17 h / 20 °C
6.1: Iodine monochloride; calcium carbonate / methanol; water / 20 °C
With
hydrogenchloride; sulfuric acid; water; hydrogen; Iodine monochloride; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; calcium carbonate; potassium iodide; sodium nitrite;
palladium on activated charcoal;
In
1,4-dioxane; methanol; water; N,N-dimethyl-formamide;