C₄₆H₅₇N₃O₉S

Base Information

Chemical Name:C₄₆H₅₇N₃O₉S
CAS No.:1599485-66-1
Molecular Formula:C₄₆H₅₇N₃O₉S
Molecular Weight:828.039
Hs Code.:

C<sub>46</sub>H<sub>57</sub>N<sub>3</sub>O<sub>9</sub>S

Synonyms:C₄₆H₅₇N₃O₉S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₆H₅₇N₃O₉S

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Technology Process of C₄₆H₅₇N₃O₉S

There total 6 articles about C₄₆H₅₇N₃O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1599485-64-9
C₅₃H₆₃N₃O₉S

: 1599485-66-1
C₄₆H₅₇N₃O₉S

Guidance literature:: With lithium hydroxide; In water; isopropyl alcohol; at 20 ℃; for 1h;

Reference yield:

: 830-79-5
2,4,6-trimethoxybenzaldehyde

: 1599485-66-1
C₄₆H₅₇N₃O₉S

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium cyanoborohydride / dichloromethane; methanol / 1.5 h / Molecular sieve

2.1: dicyclohexyl-carbodiimide; 2,4,6-trimethyl-pyridine; ethyl cyanoglyoxylate-2-oxime / dichloromethane / 3 h / 20 °C

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 0.2 h / 20 °C / Molecular sieve

4.1: dichloromethane / Molecular sieve

4.2: 22 h / 20 °C

5.1: lithium hydroxide / water; isopropyl alcohol / 1 h / 20 °C

With 2,4,6-trimethyl-pyridine; sodium cyanoborohydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; ethyl cyanoglyoxylate-2-oxime; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; isopropyl alcohol;

Reference yield:

: 1599485-62-7
N-boc-N’-tmob-ethylenediamine

: 1599485-66-1
C₄₆H₅₇N₃O₉S

Guidance literature:: Multi-step reaction with 4 steps

1.1: dicyclohexyl-carbodiimide; 2,4,6-trimethyl-pyridine; ethyl cyanoglyoxylate-2-oxime / dichloromethane / 3 h / 20 °C

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 0.2 h / 20 °C / Molecular sieve

3.1: dichloromethane / Molecular sieve

3.2: 22 h / 20 °C

4.1: lithium hydroxide / water; isopropyl alcohol / 1 h / 20 °C

With 2,4,6-trimethyl-pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; ethyl cyanoglyoxylate-2-oxime; lithium hydroxide; In tetrahydrofuran; dichloromethane; water; isopropyl alcohol;