C₁₈H₁₉ClN₂O₅S

Base Information

Chemical Name:C₁₈H₁₉ClN₂O₅S
CAS No.:1408186-99-1
Molecular Formula:C₁₈H₁₉ClN₂O₅S
Molecular Weight:410.878
Hs Code.:

C<sub>18</sub>H<sub>19</sub>ClN<sub>2</sub>O<sub>5</sub>S

Synonyms:C₁₈H₁₉ClN₂O₅S

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Chemical Property of C₁₈H₁₉ClN₂O₅S

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Technology Process of C₁₈H₁₉ClN₂O₅S

There total 5 articles about C₁₈H₁₉ClN₂O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 1408186-93-5
ethyl (2R,3S)-3-(benzyloxy)-1-((4-chlorophenyl)sulfonyl)pyrrolidine-2-carboxylate

: 1408186-99-1
C₁₈H₁₉ClN₂O₅S

Guidance literature:: With hydroxylamine potassium salt; In methanol; at 20 ℃; for 48h;
DOI:10.1016/j.ejmech.2012.08.028

Reference yield:

: 170123-25-8
3-oxo-pyrrolidine-1,2-dicarboxylic acid 1-tert-butyl ester 2-ethyl ester

: 1408186-99-1
C₁₈H₁₉ClN₂O₅S

Guidance literature:: Multi-step reaction with 5 steps

1: calcium chloride; Sucrose / water / 48 h / 30 °C / Microbiological reaction

2: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

4: triethylamine; dmap / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

5: hydroxylamine potassium salt / methanol / 48 h / 20 °C

With dmap; hydroxylamine potassium salt; tetra-(n-butyl)ammonium iodide; sodium hydride; triethylamine; trifluoroacetic acid; calcium chloride; Sucrose; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1016/j.ejmech.2012.08.028

Reference yield:

: 3783-61-7
diethyl 2-azabutane-1,4-dicarboxylate

: 1408186-99-1
C₁₈H₁₉ClN₂O₅S

Guidance literature:: Multi-step reaction with 7 steps

1: sodium hydroxide / chloroform; water / 73 h / 0 - 20 °C

2: potassium tert-butylate / toluene / 1.5 h / -10 - 0 °C / Inert atmosphere

3: calcium chloride; Sucrose / water / 48 h / 30 °C / Microbiological reaction

4: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 16 h / 0 - 20 °C / Inert atmosphere

5: trifluoroacetic acid / dichloromethane / 3 h / 20 °C

6: triethylamine; dmap / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

7: hydroxylamine potassium salt / methanol / 48 h / 20 °C

With dmap; hydroxylamine potassium salt; potassium tert-butylate; tetra-(n-butyl)ammonium iodide; sodium hydride; triethylamine; trifluoroacetic acid; calcium chloride; sodium hydroxide; Sucrose; In tetrahydrofuran; methanol; dichloromethane; chloroform; water; toluene;
DOI:10.1016/j.ejmech.2012.08.028