o-cymantrenylcarbonylbenzoic acid

Base Information

Chemical Name:o-cymantrenylcarbonylbenzoic acid
CAS No.:1224100-76-8
Molecular Formula:C₁₆H₉MnO₆
Molecular Weight:352.182
Hs Code.:

Synonyms:o-cymantrenylcarbonylbenzoic acid

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Chemical Property of o-cymantrenylcarbonylbenzoic acid

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Technology Process of o-cymantrenylcarbonylbenzoic acid

There total 1 articles about o-cymantrenylcarbonylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 85-44-9
phthalic anhydride

: 12079-65-1
cymantrene

: 1224100-76-8
o-cymantrenylcarbonylbenzoic acid

Guidance literature:: phthalic anhydride; With aluminum (III) chloride; In dichloromethane; for 0.5h; Inert atmosphere; Schlenk technique; Cooling with ice;

cymantrene; for 4.5h; Inert atmosphere; Schlenk technique; Reflux;

With hydrogenchloride; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.poly.2019.04.048

Reference yield: 81.0%

: 1224100-76-8
o-cymantrenylcarbonylbenzoic acid

: 616-38-6
carbonic acid dimethyl ester

: methyl o-cymantrenylcarbonylbenzoate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; for 13h; Reflux;
DOI:10.1016/j.poly.2019.04.048

Reference yield:

: 1224100-76-8
o-cymantrenylcarbonylbenzoic acid

: Mn(CO)3(C₅H₄CO(1,2-C₆H₄)COGLRKRLRKFRNKIKEK)

Guidance literature:: With 1-hydroxybenzotriazole; N,N-diisopropylcarbodiimide; CF₃COOH; In not given; treatment of GLRKRKRKFRNKIKEK peptide linked to polystyrene with cymantrene deriv. in presence of 5 equiv. of hydroxybenzotriazole/diimide deriv., treatment with trifluoroacetic acid in presence of different compds.; ppn. with diethyl ether at 0°C, MALDI and ESI-MS;
DOI:10.1039/b916907e