4-(10,10-dimethyl-10H-benzofuro[3,2-b]indolo[3,2,1-de]-acridine-8-yl)-N,N-diphenylaniline

Base Information

Chemical Name:4-(10,10-dimethyl-10H-benzofuro[3,2-b]indolo[3,2,1-de]-acridine-8-yl)-N,N-diphenylaniline
CAS No.:1616737-04-2
Molecular Formula:C₄₅H₃₂N₂O
Molecular Weight:616.762
Hs Code.:

Synonyms:4-(10,10-dimethyl-10H-benzofuro[3,2-b]indolo[3,2,1-de]-acridine-8-yl)-N,N-diphenylaniline

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Chemical Property of 4-(10,10-dimethyl-10H-benzofuro[3,2-b]indolo[3,2,1-de]-acridine-8-yl)-N,N-diphenylaniline

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Technology Process of 4-(10,10-dimethyl-10H-benzofuro[3,2-b]indolo[3,2,1-de]-acridine-8-yl)-N,N-diphenylaniline

There total 5 articles about 4-(10,10-dimethyl-10H-benzofuro[3,2-b]indolo[3,2,1-de]-acridine-8-yl)-N,N-diphenylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1616736-39-0
8-chloro-10,10-dimethyl-10H-benzofuro[3,2-b]indolo[3,2,1-de]-acridine

: 201802-67-7
4-(diphenylamino)phenyl boronic acid

: 1616737-04-2
4-(10,10-dimethyl-10H-benzofuro[3,2-b]indolo[3,2,1-de]-acridine-8-yl)-N,N-diphenylaniline

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; In toluene; for 8h; Reflux;

Reference yield:

: 1616736-38-9
2-(2-(5H-benzofuro[3,2-c]carbazole 5-yl)-5-chlorophenyl)propane-2-ol

: 1616737-04-2
4-(10,10-dimethyl-10H-benzofuro[3,2-b]indolo[3,2,1-de]-acridine-8-yl)-N,N-diphenylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: methanesulfonic acid / toluene / 3 h / Reflux

2: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / toluene / 8 h / Reflux

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; methanesulfonic acid; palladium diacetate; In toluene;

Reference yield:

: 27007-53-0
methyl-2-bromo-5-chlorobenzoate

: 1616737-04-2
4-(10,10-dimethyl-10H-benzofuro[3,2-b]indolo[3,2,1-de]-acridine-8-yl)-N,N-diphenylaniline

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; potassium phosphate / 5,5-dimethyl-1,3-cyclohexadiene / 12 h / Reflux

2: tetrahydrofuran / 12 h / 0 - 20 °C

3: methanesulfonic acid / toluene / 3 h / Reflux

4: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / toluene / 8 h / Reflux

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; copper(l) iodide; methanesulfonic acid; palladium diacetate; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; toluene;