4-methoxyphenyl 4-(2-tetrahydropyranyl)benzyl ketoxime

Base Information

Chemical Name:4-methoxyphenyl 4-(2-tetrahydropyranyl)benzyl ketoxime
CAS No.:120402-01-9
Molecular Formula:C₂₀H₂₃NO₄
Molecular Weight:341.407
Hs Code.:

Synonyms:4-methoxyphenyl 4-(2-tetrahydropyranyl)benzyl ketoxime

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Chemical Property of 4-methoxyphenyl 4-(2-tetrahydropyranyl)benzyl ketoxime

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Technology Process of 4-methoxyphenyl 4-(2-tetrahydropyranyl)benzyl ketoxime

There total 3 articles about 4-methoxyphenyl 4-(2-tetrahydropyranyl)benzyl ketoxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 120401-99-2
1-(4'-methoxyphenyl)-2-<4'-(tetrahydro-2''H-pyran-2''-yloxy)phenyl>ethanone

: 120402-01-9
4-methoxyphenyl 4-(2-tetrahydropyranyl)benzyl ketoxime

Guidance literature:: With potassium hydroxide; hydroxylamine hydrochloride; In tetrahydrofuran; ethanol; Ambient temperature;
DOI:10.1248/cpb.36.3142

Reference yield:

: 110-87-2
3,4-dihydro-2H-pyran

: 120402-01-9
4-methoxyphenyl 4-(2-tetrahydropyranyl)benzyl ketoxime

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / p-toluenesulfonic acid monohydrate / 6 h / Ambient temperature

2: 70 percent / hydroxylamine hidrochloride, KOH / tetrahydrofuran; ethanol / Ambient temperature

With potassium hydroxide; hydroxylamine hydrochloride; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol;
DOI:10.1248/cpb.36.3142

Reference yield:

: 13619-63-1
2-(4-hydroxyphenyl)-4-methoxyacetophenone

: 120402-01-9
4-methoxyphenyl 4-(2-tetrahydropyranyl)benzyl ketoxime

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / p-toluenesulfonic acid monohydrate / 6 h / Ambient temperature

2: 70 percent / hydroxylamine hidrochloride, KOH / tetrahydrofuran; ethanol / Ambient temperature

With potassium hydroxide; hydroxylamine hydrochloride; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol;
DOI:10.1248/cpb.36.3142