9-O-acetyl-12,13-dihydro-13-hydroxy-12-[(3-phenylpropyl)amino]midecamycin 12-N,13-O-cyclic carbamate

Base Information

• Chemical Name: 9-O-acetyl-12,13-dihydro-13-hydroxy-12-[(3-phenylpropyl)amino]midecamycin 12-N,13-O-cyclic carbamate
• CAS No.: 1033498-92-8
• Molecular Formula: C₅₃H₈₀N₂O₁₈
• Molecular Weight: 1033.22
• Mol file: 1033498-92-8.mol

Synonyms:9-O-acetyl-12,13-dihydro-13-hydroxy-12-[(3-phenylpropyl)amino]midecamycin 12-N,13-O-cyclic carbamate

Chemical Property of 9-O-acetyl-12,13-dihydro-13-hydroxy-12-[(3-phenylpropyl)amino]midecamycin 12-N,13-O-cyclic carbamate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 9-O-acetyl-12,13-dihydro-13-hydroxy-12-[(3-phenylpropyl)amino]midecamycin 12-N,13-O-cyclic carbamate

There total 1 articles about 9-O-acetyl-12,13-dihydro-13-hydroxy-12-[(3-phenylpropyl)amino]midecamycin 12-N,13-O-cyclic carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

9-O-acetyl-12,13-dihydro-13-hydroxy-12-[(3-phenylpropyl)amino]midecamycin 18-dimethylacetal 12-N,13-O-cyclic carbamate (1033498-89-3) → 9-O-acetyl-12,13-dihydro-13-hydroxy-12-[(3-phenylpropyl)amino]midecamycin 12-N,13-O-cyclic carbamate (1033498-92-8)

Guidance literature:

With Difluoroacetic acid; In water; acetonitrile; at 20 - 35 ℃; for 26.5h;

DOI:10.1016/j.bmc.2008.01.027

upstream raw materials:

9-O-acetyl-12,13-dihydro-13-hydroxy-12-[(3-phenylpropyl)amino]midecamycin 18-dimethylacetal 12-N,13-O-cyclic carbamate