(S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-2-(4-methoxy-benzyloxy)-butyric acid methyl ester

Base Information

Chemical Name:(S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-2-(4-methoxy-benzyloxy)-butyric acid methyl ester
CAS No.:180285-50-1
Molecular Formula:C₃₀H₃₈O₅Si
Molecular Weight:506.714
Hs Code.:

Synonyms:(S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-2-(4-methoxy-benzyloxy)-butyric acid methyl ester

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Chemical Property of (S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-2-(4-methoxy-benzyloxy)-butyric acid methyl ester

Chemical Property:

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Technology Process of (S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-2-(4-methoxy-benzyloxy)-butyric acid methyl ester

There total 6 articles about (S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-2-(4-methoxy-benzyloxy)-butyric acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 180285-50-1
(S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-2-(4-methoxy-benzyloxy)-butyric acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / PPTS / dimethylformamide / 2 h / 55 °C / 25 Torr

2: i-Bu₂AlH / CH₂Cl₂ / 2 h / -78 °C

3: pyridinium dichromate / dimethylformamide / 96 h / Ambient temperature

4: diethyl ether; CHCl₃

With dipyridinium dichromate; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; In diethyl ether; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(96)00804-0

Reference yield:

: tert-Butyl-(2-methylene-butoxy)-diphenyl-silane

: 180285-50-1
(S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-2-(4-methoxy-benzyloxy)-butyric acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: AD-mix-β / 2-methyl-propan-2-ol; H2O / 0 °C

2: 98 percent / PPTS / dimethylformamide / 2 h / 55 °C / 25 Torr

3: i-Bu₂AlH / CH₂Cl₂ / 2 h / -78 °C

4: pyridinium dichromate / dimethylformamide / 96 h / Ambient temperature

5: diethyl ether; CHCl₃

With dipyridinium dichromate; AD-mix-β; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; In diethyl ether; dichloromethane; chloroform; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/0040-4039(96)00804-0

Reference yield:

: 155987-99-8
(R)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-butane-1,2-diol

: 180285-50-1
(S)-2-(tert-Butyl-diphenyl-silanyloxymethyl)-2-(4-methoxy-benzyloxy)-butyric acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / PPTS / dimethylformamide / 2 h / 55 °C / 25 Torr

2: i-Bu₂AlH / CH₂Cl₂ / 2 h / -78 °C

3: pyridinium dichromate / dimethylformamide / 96 h / Ambient temperature

4: diethyl ether; CHCl₃

With dipyridinium dichromate; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; In diethyl ether; dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1016/0040-4039(96)00804-0