2-Propen-1-amine, 3-(3,4-dichlorophenyl)-, (2E)-

Base Information

Chemical Name:2-Propen-1-amine, 3-(3,4-dichlorophenyl)-, (2E)-
CAS No.:83665-76-3
Molecular Formula:C₉H₉Cl₂N
Molecular Weight:202.083
Hs Code.:
DSSTox Substance ID:DTXSID801255416

Synonyms:83665-76-3;2-Propen-1-amine, 3-(3,4-dichlorophenyl)-, (2E)-;DTXSID801255416;3-(3,4-dichlorophenyl)prop-2-en-1-amine;(E)-3-(3,4-Dichlorophenyl)prop-2-en-1-amine;EN300-1246786;(2E)-3-(3,4-Dichlorophenyl)-2-propen-1-amine

Suppliers and Price of 2-Propen-1-amine, 3-(3,4-dichlorophenyl)-, (2E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2-Propen-1-amine, 3-(3,4-dichlorophenyl)-, (2E)-

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:201.0112047
Heavy Atom Count:12
Complexity:159

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=C(C=C1C=CCN)Cl)Cl
Isomeric SMILES:C1=CC(=C(C=C1/C=C/CN)Cl)Cl

Technology Process of 2-Propen-1-amine, 3-(3,4-dichlorophenyl)-, (2E)-

There total 2 articles about 2-Propen-1-amine, 3-(3,4-dichlorophenyl)-, (2E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 83665-60-5
(E)-2-(3-(3,4-dichlorophenyl)allyl)isoindoline-1,3-dione

: 83665-76-3
(E)-3-(3,4-dichlorophenyl)prop-2-en-1-amine

Guidance literature:: With hydrazine hydrate; In ethanol; Reflux;
DOI:10.1016/j.bmc.2009.05.085

Reference yield:

: 20555-91-3
3,4-dichloroiodobenzene

: 83665-76-3
(E)-3-(3,4-dichlorophenyl)prop-2-en-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / palladium acetate, triethylamine / 18 h / 100 °C

2: 1.) hydrazine hydrate, 2.) NaOH / 1.) ethanol, reflux, 2.) water

With sodium hydroxide; palladium diacetate; hydrazine hydrate; triethylamine;
DOI:10.1021/jo00148a033

Reference yield: 74.0%

: 83665-76-3
(E)-3-(3,4-dichlorophenyl)prop-2-en-1-amine

: 103790-23-4
3-(4-methanesulphonylamidophenyl)propanoic acid

: 1194838-88-4
N-(3,4-dichlorocinnamyl)-3-(4-(methylsulfonamido)-phenyl)propanamide

Guidance literature:: 3-(4-methanesulphonylamidophenyl)propanoic acid; With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 0 ℃; for 0.75h;

(E)-3-(3,4-dichlorophenyl)prop-2-en-1-amine; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1016/j.bmc.2009.05.085