(2Z,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)-2-methoxy-1-phenylocta-2,5-dien-1-ol

Base Information

Chemical Name:(2Z,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)-2-methoxy-1-phenylocta-2,5-dien-1-ol
CAS No.:1000153-26-3
Molecular Formula:C₃₃H₄₀O₆
Molecular Weight:532.677
Hs Code.:

Synonyms:(2Z,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)-2-methoxy-1-phenylocta-2,5-dien-1-ol

Suppliers and Price of (2Z,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)-2-methoxy-1-phenylocta-2,5-dien-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2Z,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)-2-methoxy-1-phenylocta-2,5-dien-1-ol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2Z,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)-2-methoxy-1-phenylocta-2,5-dien-1-ol

There total 3 articles about (2Z,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)-2-methoxy-1-phenylocta-2,5-dien-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: (PMBOCH₂CH₂C)2

: 133350-18-2
(R,S)-2-methoxy-1-phenyl-buta-2,3-dien-1-ol

: 1000153-26-3
(2Z,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)-2-methoxy-1-phenylocta-2,5-dien-1-ol

Guidance literature:: (PMBOCH₂CH₂C)2; With titanium(IV) isopropylate; cyclopentylmagnesium chloride; In diethyl ether; hexane; toluene; at -78 - -30 ℃;

(R,S)-2-methoxy-1-phenyl-buta-2,3-dien-1-ol; With n-butyllithium; In diethyl ether; hexane; toluene; at -78 - 0 ℃; Further stages.;
DOI:10.1039/b708256h

Reference yield: 87.0%

: (PMBOCH₂CH₂C)2

: C₁₁H₁₁O₂^(1-)*Li⁽¹⁺⁾

: 1000153-26-3
(2Z,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)-2-methoxy-1-phenylocta-2,5-dien-1-ol

Guidance literature:: (PMBOCH₂CH₂C)2; With titanium(IV) isopropylate; cyclopentylmagnesium chloride; In diethyl ether; toluene; at -78 - -30 ℃; for 2h;

C₁₁H₁₁O₂^(1-)*Li⁽¹⁺⁾; In diethyl ether; hexane; toluene; at -78 - 0 ℃; for 3h;

With water; ammonium chloride; In diethyl ether; hexane; toluene; at 0 - 20 ℃; Further stages.;
DOI:10.1016/j.tet.2008.02.015

Reference yield:

: (PMBOCH₂CH₂C)2

: 133350-18-2
(R,S)-2-methoxy-1-phenyl-buta-2,3-dien-1-ol

: 1000153-26-3
(2Z,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)-2-methoxy-1-phenylocta-2,5-dien-1-ol

: (2E,5Z)-8-(4-methoxybenzyloxy)-5-(2-(4-methoxybenzyloxy)ethyl)-2-methoxy-1-phenylocta-2,5-dien-1-ol

Guidance literature:: (PMBOCH₂CH₂C)2; With titanium(IV) isopropylate; cyclopentylmagnesium chloride; In diethyl ether; toluene; at -30 ℃; for 1h;

(R,S)-2-methoxy-1-phenyl-buta-2,3-dien-1-ol; With n-butyllithium; In diethyl ether; hexane; toluene; at -78 - 0 ℃; for 3h; Further stages.;
DOI:10.1016/j.tet.2008.03.086