(Z)-3,4-dimethoxybenzaldehyde oxime

Base Information

Chemical Name:(Z)-3,4-dimethoxybenzaldehyde oxime
CAS No.:1195641-91-8
Molecular Formula:C₉H₁₁NO₃
Molecular Weight:181.191
Hs Code.:

Synonyms:(Z)-3,4-dimethoxybenzaldehyde oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-3,4-dimethoxybenzaldehyde oxime

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Technology Process of (Z)-3,4-dimethoxybenzaldehyde oxime

There total 4 articles about (Z)-3,4-dimethoxybenzaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 24393-47-3
ethyl (E)-2-cyano-3-(3,4-dimethoxyphenyl)-2-propenoate

: 1195641-91-8
(Z)-3,4-dimethoxybenzaldehyde oxime

Guidance literature:: With hydroxylamine hydrochloride; sodium carbonate; In methanol; water; at 100 ℃; for 1h; stereoselective reaction;
DOI:10.1016/j.molstruc.2020.128699

Reference yield:

: 120-14-9
3,4-dimethoxy-benzaldehyde

: 1195641-91-8
(Z)-3,4-dimethoxybenzaldehyde oxime

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / ethanol / 80 - 85 °C

2: sodium carbonate; hydroxylamine hydrochloride / water; methanol / 1 h / 100 °C

With piperidine; hydroxylamine hydrochloride; sodium carbonate; In methanol; ethanol; water;
DOI:10.1016/j.molstruc.2020.128699