4-Methyl-N-((1S,2S,6R)-1,10,10-trimethyl-3-oxa-5-aza-tricyclo[5.2.1.0^2,6]dec-4-en-4-ylmethyl)-benzenesulfonamide

Base Information

• Chemical Name: 4-Methyl-N-((1S,2S,6R)-1,10,10-trimethyl-3-oxa-5-aza-tricyclo[5.2.1.0^2,6]dec-4-en-4-ylmethyl)-benzenesulfonamide
• CAS No.: 144397-21-7
• Molecular Formula: C₁₉H₂₆N₂O₃S
• Molecular Weight: 362.493

Synonyms:4-Methyl-N-((1S,2S,6R)-1,10,10-trimethyl-3-oxa-5-aza-tricyclo[5.2.1.0^2,6]dec-4-en-4-ylmethyl)-benzenesulfonamide

Chemical Property of 4-Methyl-N-((1S,2S,6R)-1,10,10-trimethyl-3-oxa-5-aza-tricyclo[5.2.1.0^2,6]dec-4-en-4-ylmethyl)-benzenesulfonamide

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Technology Process of 4-Methyl-N-((1S,2S,6R)-1,10,10-trimethyl-3-oxa-5-aza-tricyclo[5.2.1.0^2,6]dec-4-en-4-ylmethyl)-benzenesulfonamide

There total 1 articles about 4-Methyl-N-((1S,2S,6R)-1,10,10-trimethyl-3-oxa-5-aza-tricyclo[5.2.1.0^2,6]dec-4-en-4-ylmethyl)-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-N-p-tolylsulphonylaminoacetimidate hydrochloride (144397-30-8) + (1S,2S,3R)-3-Amino-1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-ol (1925-44-6,1925-45-7,24054-01-1,25050-53-7,29900-93-4,30009-19-9,32232-11-4,41719-73-7,51773-76-3,52729-45-0,52729-46-1,99341-59-0) → 4-Methyl-N-((1S,2S,6R)-1,10,10-trimethyl-3-oxa-5-aza-tricyclo[5.2.1.02,6]dec-4-en-4-ylmethyl)-benzenesulfonamide (144397-21-7)

Guidance literature:

With triethylamine; In dichloromethane; for 20h;

DOI:10.1080/00397919208021650

upstream raw materials:

2-N-p-tolylsulphonylaminoacetimidate hydrochloride

(1S,2S,3R)-3-Amino-1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-ol

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