C₃₀H₃₅NO₇SSi

Base Information

• Chemical Name: C₃₀H₃₅NO₇SSi
• CAS No.: 1312542-05-4
• Molecular Formula: C₃₀H₃₅NO₇SSi
• Molecular Weight: 581.762
• Mol file: 1312542-05-4.mol

Synonyms:C₃₀H₃₅NO₇SSi

Chemical Property of C₃₀H₃₅NO₇SSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₃₀H₃₅NO₇SSi

There total 1 articles about C₃₀H₃₅NO₇SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

C14H24O3Si (1199940-92-5) + C16H11NO4S (1312542-01-0) → C30H35NO7SSi (1312542-05-4)

Guidance literature:

In dichloromethane; at 25 ℃; for 24h; stereoselective reaction; Inert atmosphere;

DOI:10.1021/ol201095b

Reference yield: 94.0%

C30H35NO7SSi (1312542-05-4) → C28H35NO6SSi (1312542-18-9)

Guidance literature:

With diisobutylaluminium hydride; In dichloromethane; at -30 ℃; for 0.5h; regioselective reaction; Inrtert atmosphere;

DOI:10.1021/ol201095b

Reference yield:

C30H35NO7SSi (1312542-05-4) → C30H37NO3Si (1312542-26-9)

Guidance literature:

Multi-step reaction with 8 steps

1.1: diisobutylaluminium hydride / dichloromethane / 0.5 h / -30 °C / Inrtert atmosphere

2.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 - 25 °C

3.1: N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide / tetrahydrofuran / 0.33 h / -20 °C

3.2: 0.5 h / -20 - 25 °C

4.1: hydrogenchloride / 72 h / 120 °C / Inert atmosphere; Molecular sieve

5.1: pyridine / 6 h / 25 °C

6.1: 2 h / 180 °C / vacuum

7.1: tetrahydrofuran / 0.5 h / -30 °C

8.1: potassium hexamethylsilazane / diethylene glycol dimethyl ether; toluene / 1 h / 95 °C / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide; potassium hexamethylsilazane; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane; diethylene glycol dimethyl ether; toluene;

DOI:10.1021/ol201095b

upstream raw materials:

C₁₄H₂₄O₃Si

C₁₆H₁₁NO₄S

Downstream raw materials:

C₂₈H₃₅NO₆SSi

C₃₄H₄₉NO₆SSi₂

C₂₉H₄₇NO₄Si₂

C₂₀H₂₅NO₄