(benzyloxy-2 trifluoromethyl-5 phenyl)-1 <(tert.butoxycarbonyl) amino>-3 azetidinone-2 (3-S)

Base Information

Chemical Name:(benzyloxy-2 trifluoromethyl-5 phenyl)-1 <(tert.butoxycarbonyl) amino>-3 azetidinone-2 (3-S)
CAS No.:117901-18-5
Molecular Formula:C₂₂H₂₃F₃N₂O₄
Molecular Weight:436.431
Hs Code.:

Synonyms:(benzyloxy-2 trifluoromethyl-5 phenyl)-1 <(tert.butoxycarbonyl) amino>-3 azetidinone-2 (3-S)

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Chemical Property of (benzyloxy-2 trifluoromethyl-5 phenyl)-1 <(tert.butoxycarbonyl) amino>-3 azetidinone-2 (3-S)

Chemical Property:

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Technology Process of (benzyloxy-2 trifluoromethyl-5 phenyl)-1 <(tert.butoxycarbonyl) amino>-3 azetidinone-2 (3-S)

There total 1 articles about (benzyloxy-2 trifluoromethyl-5 phenyl)-1 <(tert.butoxycarbonyl) amino>-3 azetidinone-2 (3-S) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 117901-13-0
N-(benzyloxy-2 trifluoromethyl-5 phenyl) <(tert.butoxycarbonyl) amino>-2 hydroxy-3 propionamide (2-S)

: 117901-19-6
N-(benzyloxy-2 trifluoromethyl-5 phenyl)-1 <(tert.butoxycarbonyl) amino>-2 propen-2 amide

: 117901-20-9
N-(benzyloxy-2 trifluoromethyl-5 phenyl) (tert.butoxycarbonyl)-1 aziridine-2 carboxamide (2-S)

: 117901-18-5
(benzyloxy-2 trifluoromethyl-5 phenyl)-1 <(tert.butoxycarbonyl) amino>-3 azetidinone-2 (3-S)

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 1.) 0 deg C, 1 h; 2.) r.t., 15 h;

Reference yield: 48.0%

: 117901-18-5
(benzyloxy-2 trifluoromethyl-5 phenyl)-1 <(tert.butoxycarbonyl) amino>-3 azetidinone-2 (3-S)

: 117901-24-3
<(tert.butoxycarbonyl)amino>-3 (hydroxy-2 trifluoromethyl-5 phenyl)-1 azetidinone-2 (3-S)

Guidance literature:: With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; for 1h; under 1200 Torr;

Reference yield:

: 117901-18-5
(benzyloxy-2 trifluoromethyl-5 phenyl)-1 <(tert.butoxycarbonyl) amino>-3 azetidinone-2 (3-S)

: 117901-34-5
<(tert.butoxycarbonyl)amino>-3 (hydroxy-2 nitro-3 trifluoromethyl-5 phenyl)-1 azetidinone-2 (3-S)

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / hydrogen / black palladium/C / tetrahydrofuran; methanol / 1 h / 1200 Torr

2: 56 percent / HNO₃, acetic acid / 1 h / Ambient temperature

With hydrogen; nitric acid; acetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol;