2-(4-(2-(2-(2-aminoethoxy)ethoxy)ethoxy)-3,5-dichlorophenylamino)benzoic acid trifluoroacetate

Base Information

• Chemical Name: 2-(4-(2-(2-(2-aminoethoxy)ethoxy)ethoxy)-3,5-dichlorophenylamino)benzoic acid trifluoroacetate
• CAS No.: 1346597-64-5
• Molecular Formula: C₂HF₃O₂*C₁₉H₂₂Cl₂N₂O₅
• Molecular Weight: 543.324

Synonyms:2-(4-(2-(2-(2-aminoethoxy)ethoxy)ethoxy)-3,5-dichlorophenylamino)benzoic acid trifluoroacetate

Chemical Property of 2-(4-(2-(2-(2-aminoethoxy)ethoxy)ethoxy)-3,5-dichlorophenylamino)benzoic acid trifluoroacetate

Chemical Property:

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Technology Process of 2-(4-(2-(2-(2-aminoethoxy)ethoxy)ethoxy)-3,5-dichlorophenylamino)benzoic acid trifluoroacetate

There total 2 articles about 2-(4-(2-(2-(2-aminoethoxy)ethoxy)ethoxy)-3,5-dichlorophenylamino)benzoic acid trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl 2-(2-(2-hydroxyethoxy)ethoxy)ethylcarbamate (139115-92-7) → 2-(4-(2-(2-(2-aminoethoxy)ethoxy)ethoxy)-3,5-dichlorophenylamino)benzoic acid trifluoroacetate (1346597-64-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 1,1'-azodicarbonyl-dipiperidine; triphenylphosphine / tetrahydrofuran / 96 h / 20 °C / Inert atmosphere

2: dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

With triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; dichloromethane;

Reference yield:

tert-butyl 2-(4-hydroxy-3,5-dichlorophenylamino)benzoate (851962-03-3) → 2-(4-(2-(2-(2-aminoethoxy)ethoxy)ethoxy)-3,5-dichlorophenylamino)benzoic acid trifluoroacetate (1346597-64-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 1,1'-azodicarbonyl-dipiperidine; triphenylphosphine / tetrahydrofuran / 96 h / 20 °C / Inert atmosphere

2: dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

With triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; dichloromethane;

Reference yield: 52.0%

fluorescein isothiocyanate (3326-32-7,27072-45-3) + 2-(4-(2-(2-(2-aminoethoxy)ethoxy)ethoxy)-3,5-dichlorophenylamino)benzoic acid trifluoroacetate (1346597-64-5) → 2-(3,5-dichloro-4-(2-(2-(2-(3-(3',6'-dihydroxy-3-oxo-3H-spiro[isobenzofuran-1,9'-xanthene]-5-yl)thioureido)ethoxy)ethoxy)ethoxy)phenylamino)benzoic acid (1346597-65-6)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 16h; Inert atmosphere;

upstream raw materials:

tert-butyl 2-(2-(2-hydroxyethoxy)ethoxy)ethylcarbamate

tert-butyl 2-(4-hydroxy-3,5-dichlorophenylamino)benzoate

Downstream raw materials:

2-(3,5-dichloro-4-(2-(2-(2-(3-(3',6'-dihydroxy-3-oxo-3H-spiro[isobenzofuran-1,9'-xanthene]-5-yl)thioureido)ethoxy)ethoxy)ethoxy)phenylamino)benzoic acid

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