3-hydroxy-6-methyl-2-methylene-N-phenyl-4-<(trimethylsilyl)oxy>heptanamide

Base Information

Chemical Name:3-hydroxy-6-methyl-2-methylene-N-phenyl-4-<(trimethylsilyl)oxy>heptanamide
CAS No.:103633-68-7
Molecular Formula:C₁₈H₂₉NO₃Si
Molecular Weight:335.519
Hs Code.:

Synonyms:3-hydroxy-6-methyl-2-methylene-N-phenyl-4-<(trimethylsilyl)oxy>heptanamide

Suppliers and Price of 3-hydroxy-6-methyl-2-methylene-N-phenyl-4-<(trimethylsilyl)oxy>heptanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-hydroxy-6-methyl-2-methylene-N-phenyl-4-<(trimethylsilyl)oxy>heptanamide

Chemical Property:

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Technology Process of 3-hydroxy-6-methyl-2-methylene-N-phenyl-4-<(trimethylsilyl)oxy>heptanamide

There total 6 articles about 3-hydroxy-6-methyl-2-methylene-N-phenyl-4-<(trimethylsilyl)oxy>heptanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 103633-66-5
6-methyl-N-phenyl-2-<(phenylseleno)methyl>-4-<(trimethylsilyl)oxy>-2-heptenamide

: 103633-68-7
3-hydroxy-6-methyl-2-methylene-N-phenyl-4-<(trimethylsilyl)oxy>heptanamide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 ℃; for 1h;
DOI:10.1016/S0040-4039(00)94941-4 DOI:10.1021/jo00262a020

Reference yield:

: 103633-60-9
4-hydroxy-6-methyl-2-methylene-N-phenyl-3-(phenylsulfonyl)heptanamide

: 103633-68-7
3-hydroxy-6-methyl-2-methylene-N-phenyl-4-<(trimethylsilyl)oxy>heptanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent

2: 91 percent / NaBH₄ / ethanol; tetrahydrofuran / 2 h / Ambient temperature

3: 98 percent / MCPBA / CH₂Cl₂ / 1 h / -78 °C

With sodium tetrahydroborate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jo00262a020

Reference yield:

: 103633-63-2
6-methyl-2-methylene-N-phenyl-3-(phenylsulfonyl)-4-<(trimethylsilyl)oxy>heptanamide

: 103633-68-7
3-hydroxy-6-methyl-2-methylene-N-phenyl-4-<(trimethylsilyl)oxy>heptanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / NaBH₄ / ethanol; tetrahydrofuran / 2 h / Ambient temperature

2: 98 percent / MCPBA / CH₂Cl₂ / 1 h / -78 °C

With sodium tetrahydroborate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1021/jo00262a020