7,7-ethylenedioxy-4-[N-(2-methylprop-2-yloxycarbonyl)amino]-2-oxoundecan-1-yl phenyl sulfone

Base Information

Chemical Name:7,7-ethylenedioxy-4-[N-(2-methylprop-2-yloxycarbonyl)amino]-2-oxoundecan-1-yl phenyl sulfone
CAS No.:956620-40-9
Molecular Formula:C₂₄H₃₇NO₇S
Molecular Weight:483.626
Hs Code.:

Synonyms:7,7-ethylenedioxy-4-[N-(2-methylprop-2-yloxycarbonyl)amino]-2-oxoundecan-1-yl phenyl sulfone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7,7-ethylenedioxy-4-[N-(2-methylprop-2-yloxycarbonyl)amino]-2-oxoundecan-1-yl phenyl sulfone

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Technology Process of 7,7-ethylenedioxy-4-[N-(2-methylprop-2-yloxycarbonyl)amino]-2-oxoundecan-1-yl phenyl sulfone

There total 1 articles about 7,7-ethylenedioxy-4-[N-(2-methylprop-2-yloxycarbonyl)amino]-2-oxoundecan-1-yl phenyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 7,7-ethylenedioxy-2-hydroxy-4-[N-(2-methylprop-2-yloxycarbonyl)amino]undecan-1-yl phenyl sulfone

: 956620-40-9
7,7-ethylenedioxy-4-[N-(2-methylprop-2-yloxycarbonyl)amino]-2-oxoundecan-1-yl phenyl sulfone

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1039/b708910d

Reference yield:

: 956620-40-9
7,7-ethylenedioxy-4-[N-(2-methylprop-2-yloxycarbonyl)amino]-2-oxoundecan-1-yl phenyl sulfone

: 141936-92-7
1-Benzenesulfonyl-3-(5-butyl-3,4-dihydro-2H-pyrrol-2-yl)-propan-2-one

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1039/c39920000538

Reference yield:

: 956620-40-9
7,7-ethylenedioxy-4-[N-(2-methylprop-2-yloxycarbonyl)amino]-2-oxoundecan-1-yl phenyl sulfone

: 141936-94-9
(1RS,2RS,5SR)-1-butyl-2-phenylsulfonyl-8-(2,2,2-trichloroethoxycarbonyl)-8-azabicyclo[3.2.1]octan-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: CF₃COOH / CH₂Cl₂ / 3 h / 0 - 20 °C

2: Et₃N / CH₂Cl₂ / 12 h / -78 °C

With triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1039/c39920000538