phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside

Base Information

Chemical Name:phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside
CAS No.:1192142-81-6
Molecular Formula:C₉₀H₉₅NO₁₆S
Molecular Weight:1478.81
Hs Code.:

phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside

Synonyms:phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside

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Chemical Property of phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside

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Technology Process of phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside

There total 1 articles about phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1192142-77-0
phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-3,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside

: 1192142-81-6
phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside

Guidance literature:: With acetic acid; zinc; In ethyl acetate; for 0.5h; Inert atmosphere; Microwave irradiation;
DOI:10.1016/j.tet.2009.07.080

Reference yield: 98.0%

: 1192142-81-6
phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside

: 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-D-mannopyranose

Guidance literature:: With N-Bromosuccinimide; water; In acetone; at 20 ℃; for 0.5h;
DOI:10.1016/j.tet.2009.07.080

Reference yield: 41.0%

: 1192142-81-6
phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside

: 125760-26-1
N-Fmoc serine phenacyl ester

: 1192143-24-0
N-(9-fluorenylmethoxycarbonyl)-O-[2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-β-D-mannopyranosyl]-L-serine phenacyl ester

: 1192142-94-1
N-(9-fluorenylmethoxycarbonyl)-O-[2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl]-L-serine phenacyl ester

Guidance literature:: phenyl 2,4,6-tri-O-benzyl-3-O-(4-methoxyphenyl)methyl-β-D-galactopyranosyl-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannnopyranoside; N-Fmoc serine phenacyl ester; With N-iodo-succinimide; In dichloromethane; at -20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

With trifluorormethanesulfonic acid; In dichloromethane; at -20 - 0 ℃; for 4.5h; optical yield given as %de; stereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tet.2009.07.080