C₅(CH₃)5RuClC₄H₂(C₆H₁₀OH)2

Base Information

Chemical Name:C₅(CH₃)5RuClC₄H₂(C₆H₁₀OH)2
CAS No.:370595-29-2
Molecular Formula:C₂₆H₃₉ClO₂Ru
Molecular Weight:520.117
Hs Code.:

C<sub>5</sub>(CH<sub>3</sub>)5RuClC<sub>4</sub>H<sub>2</sub>(C<sub>6</sub>H<sub>10</sub>OH)2

Synonyms:C₅(CH₃)5RuClC₄H₂(C₆H₁₀OH)2

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Chemical Property of C₅(CH₃)5RuClC₄H₂(C₆H₁₀OH)2

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Technology Process of C₅(CH₃)5RuClC₄H₂(C₆H₁₀OH)2

There total 1 articles about C₅(CH₃)5RuClC₄H₂(C₆H₁₀OH)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 92390-26-6
chloro(1,5-cyclooctadiene)(pentamethylcyclopentadiene)ruthenium(II)

: 78-27-3
1-Ethynylcyclohexan-1-ol

: 370595-29-2
C₅(CH₃)5RuClC₄H₂(C₆H₁₀OH)2

Guidance literature:: In tetrahydrofuran; under N2; addn. of 5 equiv. of 1-ethynylcyclohexanol to soln. of Ru complex in THF, stirred at room. temp. for 2 h; evapd. under vac., residue washed with diethyl ether, dried. under vac.;
DOI:10.1002/1521-3773(20010803)40:15<2912::AID-ANIE2912>3.0.CO;2-R

Reference yield: 90.0%

: hexafluorophosphoric acid

: 370595-29-2
C₅(CH₃)5RuClC₄H₂(C₆H₁₀OH)2

: [C₅(CH₃)5RuClC₄H(C₆H₁₀)2]⁽¹⁺⁾*PF₆^(1-)=[C₅(CH₃)5RuClC₄H(C₆H₁₀)2]PF₆

Guidance literature:: In tetrahydrofuran; water; under N2; addn. of soln. of HPF6 in H2O to soln. of Ru complex in THF at-60°C, stirred soln. was allowed to warm to room temp., kept at room temp. for 3 h; evapd. under vac., residue washed with diethyl ether, dried under vac.; elem. anal.;
DOI:10.1002/1521-3773(20010803)40:15<2912::AID-ANIE2912>3.0.CO;2-R

Reference yield: 90.0%

: tetrafluoroboric acid

: 370595-29-2
C₅(CH₃)5RuClC₄H₂(C₆H₁₀OH)2

: [C₅(CH₃)5RuClC₄H(C₆H₁₀)2]⁽¹⁺⁾*BF₄^(1-)=[C₅(CH₃)5RuClC₄H(C₆H₁₀)2]BF₄

Guidance literature:: In tetrahydrofuran; diethyl ether; under N2; addn. of soln. of HBF4 in Et2O to soln. of Ru complex in THF at -60°C, stirred soln. was allowed to warm to room temp., kept atroom temp. for 3 h; evapd. under vac., residue washed with diethyl ether, dried under vac.; elem. anal.;
DOI:10.1002/1521-3773(20010803)40:15<2912::AID-ANIE2912>3.0.CO;2-R