(3aS,7aS)-hexahydro-7a-[(4-isopropyl-2,3,5-trimethoxyphenyl)methyl]-4,4-dimethyl-2(3H)-benzofuranone

Base Information

Chemical Name:(3aS,7aS)-hexahydro-7a-[(4-isopropyl-2,3,5-trimethoxyphenyl)methyl]-4,4-dimethyl-2(3H)-benzofuranone
CAS No.:1259370-70-1
Molecular Formula:C₂₃H₃₄O₅
Molecular Weight:390.52
Hs Code.:

Synonyms:(3aS,7aS)-hexahydro-7a-[(4-isopropyl-2,3,5-trimethoxyphenyl)methyl]-4,4-dimethyl-2(3H)-benzofuranone

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Chemical Property of (3aS,7aS)-hexahydro-7a-[(4-isopropyl-2,3,5-trimethoxyphenyl)methyl]-4,4-dimethyl-2(3H)-benzofuranone

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Technology Process of (3aS,7aS)-hexahydro-7a-[(4-isopropyl-2,3,5-trimethoxyphenyl)methyl]-4,4-dimethyl-2(3H)-benzofuranone

There total 1 articles about (3aS,7aS)-hexahydro-7a-[(4-isopropyl-2,3,5-trimethoxyphenyl)methyl]-4,4-dimethyl-2(3H)-benzofuranone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1259370-71-2
(1S)-2-[2-(4-isopropyl-2,3,5-trimethoxyphenyl)methyl]-6,6-dimethyl-2-cyclohexene-1-acetic acid methyl ester

: 1259370-70-1
(3aS,7aS)-hexahydro-7a-[(4-isopropyl-2,3,5-trimethoxyphenyl)methyl]-4,4-dimethyl-2(3H)-benzofuranone

Guidance literature:: With hydrogenchloride; acetic acid; In water; at 70 ℃; for 6h; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.09.110

Reference yield: 95.0%

: 1259370-70-1
(3aS,7aS)-hexahydro-7a-[(4-isopropyl-2,3,5-trimethoxyphenyl)methyl]-4,4-dimethyl-2(3H)-benzofuranone

: 5-(((3aS,7aS)-4,4-dimethyl-2-oxohexahydrobenzofuran-7a(2H)-yl)methyl)-2-isopropyl-3-methoxycyclohexa-2,5-diene-1,4-dione

Guidance literature:: With silver(II) oxide; nitric acid; In 1,4-dioxane; water; at 5 ℃; for 8h;
DOI:10.1016/j.bmcl.2015.05.022

Reference yield: 92.0%

: 1259370-70-1
(3aS,7aS)-hexahydro-7a-[(4-isopropyl-2,3,5-trimethoxyphenyl)methyl]-4,4-dimethyl-2(3H)-benzofuranone

: 1259370-72-3
(3aS,7aS)-hexahydro-7a-[(2-iodo-4-isopropyl-2,3,5-trimethoxyphenyl)methyl]-4,4-dimethyl-2(3H)-benzofuranone

Guidance literature:: With N-iodo-succinimide; toluene-4-sulfonic acid; In 1,2-dichloro-ethane; at 45 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.09.110