1-carbamoyl-1-cyclobutane carboxylic acid

Base Information

Chemical Name:1-carbamoyl-1-cyclobutane carboxylic acid
CAS No.:219322-92-6
Molecular Formula:C₁₄H₁₇NO₃
Molecular Weight:247.294
Hs Code.:

1-<N-1(R)-phenylethyl>carbamoyl-1-cyclobutane carboxylic acid

Synonyms:1-carbamoyl-1-cyclobutane carboxylic acid

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Chemical Property of 1-carbamoyl-1-cyclobutane carboxylic acid

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Technology Process of 1-carbamoyl-1-cyclobutane carboxylic acid

There total 4 articles about 1-carbamoyl-1-cyclobutane carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 219322-91-5
ethyl 1-carbamoyl-1-cyclobutane carboxylate

: 219322-92-6
1-carbamoyl-1-cyclobutane carboxylic acid

Guidance literature:: With sodium hydroxide; In ethanol; for 1h; Ambient temperature;
DOI:10.1248/cpb.46.1710

Reference yield:

: 3779-29-1
diethyl cyclobutane-1,1-dicarboxylate

: 219322-92-6
1-carbamoyl-1-cyclobutane carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / 10 percent aq. KOH / methanol / 18 h / Ambient temperature

2: Et₃N / CHCl₃ / 0.33 h / Ambient temperature

3: CHCl₃ / 0.5 h / Ambient temperature

4: 94 percent / 20 percent aq. NaOH / ethanol / 1 h / Ambient temperature

With potassium hydroxide; sodium hydroxide; triethylamine; In methanol; ethanol; chloroform;
DOI:10.1248/cpb.46.1710

Reference yield:

: 54450-84-9
ethyl hydrogen cyclobutane-1,1-dicarboxylate

: 219322-92-6
1-carbamoyl-1-cyclobutane carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CHCl₃ / 0.33 h / Ambient temperature

2: CHCl₃ / 0.5 h / Ambient temperature

3: 94 percent / 20 percent aq. NaOH / ethanol / 1 h / Ambient temperature

With sodium hydroxide; triethylamine; In ethanol; chloroform;
DOI:10.1248/cpb.46.1710