(E)-N-(3-(2-(tert-butyldimethylsilyloxy)phenyl)propyl)buta-1,3-diene-1-sulfonamide

Base Information

Chemical Name:(E)-N-(3-(2-(tert-butyldimethylsilyloxy)phenyl)propyl)buta-1,3-diene-1-sulfonamide
CAS No.:1221740-99-3
Molecular Formula:C₁₉H₃₁NO₃SSi
Molecular Weight:381.612
Hs Code.:

Synonyms:(E)-N-(3-(2-(tert-butyldimethylsilyloxy)phenyl)propyl)buta-1,3-diene-1-sulfonamide

Suppliers and Price of (E)-N-(3-(2-(tert-butyldimethylsilyloxy)phenyl)propyl)buta-1,3-diene-1-sulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-(3-(2-(tert-butyldimethylsilyloxy)phenyl)propyl)buta-1,3-diene-1-sulfonamide

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Technology Process of (E)-N-(3-(2-(tert-butyldimethylsilyloxy)phenyl)propyl)buta-1,3-diene-1-sulfonamide

There total 7 articles about (E)-N-(3-(2-(tert-butyldimethylsilyloxy)phenyl)propyl)buta-1,3-diene-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 176697-78-2
(E)-1-(1,3-butadiene)sulfonyl chloride

: 1221740-97-1
3-(2-(tert-butyldimethylsilyloxy)phenyl)propan-1-amine

: 1221740-99-3
(E)-N-(3-(2-(tert-butyldimethylsilyloxy)phenyl)propyl)buta-1,3-diene-1-sulfonamide

Guidance literature:: With triethylamine; In tetrahydrofuran; at -20 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol1003669

Reference yield:

: 146253-19-2
3-(2-methoxyphenyl)propyl methanesulfonate

: 1221740-99-3
(E)-N-(3-(2-(tert-butyldimethylsilyloxy)phenyl)propyl)buta-1,3-diene-1-sulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: boron tribromide / dichloromethane / -20 - 20 °C / Inert atmosphere

2: sodium azide / water; N,N-dimethyl-formamide / 20 - 90 °C / Inert atmosphere

3: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

4: 10% palladium on activated carbon; hydrogen / ethanol / 20 °C

5: triethylamine / dichloromethane / -20 - 20 °C / Inert atmosphere

With 1H-imidazole; sodium azide; 10% palladium on activated carbon; hydrogen; boron tribromide; triethylamine; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/chem.201001402

Reference yield:

: 1221741-11-2
2-(3-azidopropyl)phenol

: 1221740-99-3
(E)-N-(3-(2-(tert-butyldimethylsilyloxy)phenyl)propyl)buta-1,3-diene-1-sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

2: 10% palladium on activated carbon; hydrogen / ethanol / 20 °C

3: triethylamine / dichloromethane / -20 - 20 °C / Inert atmosphere

With 1H-imidazole; 10% palladium on activated carbon; hydrogen; triethylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201001402