N-{9-[(1aR,1bS,3R,4aS,5aS)-1a-(tert-Butyl-dimethyl-silanyloxy)-4a-trimethylsilanyloxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl]-9H-purin-6-yl}-benzamide

Base Information

Chemical Name:N-{9-[(1aR,1bS,3R,4aS,5aS)-1a-(tert-Butyl-dimethyl-silanyloxy)-4a-trimethylsilanyloxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl]-9H-purin-6-yl}-benzamide
CAS No.:200931-84-6
Molecular Formula:C₂₉H₄₁N₅O₄Si₂
Molecular Weight:579.847
Hs Code.:

N-{9-[(1aR,1bS,3R,4aS,5aS)-1a-(tert-Butyl-dimethyl-silanyloxy)-4a-trimethylsilanyloxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl]-9H-purin-6-yl}-benzamide

Synonyms:N-{9-[(1aR,1bS,3R,4aS,5aS)-1a-(tert-Butyl-dimethyl-silanyloxy)-4a-trimethylsilanyloxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl]-9H-purin-6-yl}-benzamide

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Chemical Property of N-{9-[(1aR,1bS,3R,4aS,5aS)-1a-(tert-Butyl-dimethyl-silanyloxy)-4a-trimethylsilanyloxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl]-9H-purin-6-yl}-benzamide

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Technology Process of N-{9-[(1aR,1bS,3R,4aS,5aS)-1a-(tert-Butyl-dimethyl-silanyloxy)-4a-trimethylsilanyloxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl]-9H-purin-6-yl}-benzamide

There total 1 articles about N-{9-[(1aR,1bS,3R,4aS,5aS)-1a-(tert-Butyl-dimethyl-silanyloxy)-4a-trimethylsilanyloxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl]-9H-purin-6-yl}-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 10416-59-8,132255-83-5
(Z)-trimethylsilyl N-trimethylsilylacetimidate

: 4005-49-6
N-benzoyladenine

: 440114-91-0
(1aR,1bS,4aS,5aR)-1a-(tert-Butyl-dimethyl-silanyloxy)-3-methoxy-hexahydro-2-oxa-cyclopropa[a]pentalen-4a-ol

: (1aR,1bS,4aS,5aS)-1a-(tert-Butyl-dimethyl-silanyloxy)-3-methoxy-4a-trimethylsilanyloxy-octahydro-2-oxa-cyclopropa[a]pentalene

: 200931-83-5
N-{9-[(1aR,1bS,3S,4aS,5aS)-1a-(tert-Butyl-dimethyl-silanyloxy)-4a-trimethylsilanyloxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl]-9H-purin-6-yl}-benzamide

: 200931-84-6
N-{9-[(1aR,1bS,3R,4aS,5aS)-1a-(tert-Butyl-dimethyl-silanyloxy)-4a-trimethylsilanyloxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl]-9H-purin-6-yl}-benzamide

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 83 ℃; for 7h;
DOI:10.1002/hlca.19970800812

Reference yield: 95.0%

: 200931-84-6
N-{9-[(1aR,1bS,3R,4aS,5aS)-1a-(tert-Butyl-dimethyl-silanyloxy)-4a-trimethylsilanyloxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl]-9H-purin-6-yl}-benzamide

: 200931-86-8
(3'S,5'R)-N⁶-9-(2'-deoxy-3',5'-ethano-5',6'-methano-D-ribofuranosyl)adenine

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; hexane; 4 h, room t. and 1 h, 50 deg C;
DOI:10.1002/hlca.19970800812

Reference yield:

: 200931-84-6
N-{9-[(1aR,1bS,3R,4aS,5aS)-1a-(tert-Butyl-dimethyl-silanyloxy)-4a-trimethylsilanyloxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl]-9H-purin-6-yl}-benzamide

: N-(9-{(1aR,1bS,3R,4aS,5aR)-1a-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-4a-hydroxy-octahydro-2-oxa-cyclopropa[a]pentalen-3-yl}-9H-purin-6-yl)-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / Bu₄NF / tetrahydrofuran; hexane / 4 h, room t. and 1 h, 50 deg C

2: 58 percent / pyridine / 9 h / Ambient temperature

With pyridine; tetrabutyl ammonium fluoride; In tetrahydrofuran; hexane;
DOI:10.1002/hlca.19970800812