3,7-bis(dimethylamino)-5,10-diphenyl-5-thioxo-5,10-dihydrodibenzophosphorin

Base Information

Chemical Name:3,7-bis(dimethylamino)-5,10-diphenyl-5-thioxo-5,10-dihydrodibenzophosphorin
CAS No.:79462-61-6
Molecular Formula:C₂₉H₂₉N₂PS
Molecular Weight:468.602
Hs Code.:

3,7-bis(dimethylamino)-5,10-diphenyl-5-thioxo-5,10-dihydrodibenzo<b,e>phosphorin

Synonyms:3,7-bis(dimethylamino)-5,10-diphenyl-5-thioxo-5,10-dihydrodibenzophosphorin

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Chemical Property of 3,7-bis(dimethylamino)-5,10-diphenyl-5-thioxo-5,10-dihydrodibenzophosphorin

Chemical Property:

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Technology Process of 3,7-bis(dimethylamino)-5,10-diphenyl-5-thioxo-5,10-dihydrodibenzophosphorin

There total 5 articles about 3,7-bis(dimethylamino)-5,10-diphenyl-5-thioxo-5,10-dihydrodibenzophosphorin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 79462-58-1,79462-59-2,344341-56-6
3,7-bis(dimethylamino)-5,10-diphenyl-5,10-dihydrodibenzophosphorin

: 79462-61-6
3,7-bis(dimethylamino)-5,10-diphenyl-5-thioxo-5,10-dihydrodibenzophosphorin

Guidance literature:: With sulfur; In benzene; for 0.5h; Ambient temperature;

Reference yield:

: 79462-60-5
3,3'-(phenylphosphinidene)bis

: 79462-61-6
3,7-bis(dimethylamino)-5,10-diphenyl-5-thioxo-5,10-dihydrodibenzophosphorin

Guidance literature:: Multi-step reaction with 2 steps

1: 35percent HCl / 15 h / 95 °C

2: 67 percent / sulfur / benzene / 0.5 h / Ambient temperature

With hydrogenchloride; sulfur; In benzene;

Reference yield:

: 86967-66-0
(3-(dimethylamino)phenyl)magnesium bromide

: 79462-61-6
3,7-bis(dimethylamino)-5,10-diphenyl-5-thioxo-5,10-dihydrodibenzophosphorin

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / tetrahydrofuran / 4 h / Heating

2: 35percent HCl / 15 h / 95 °C

3: 67 percent / sulfur / benzene / 0.5 h / Ambient temperature

With hydrogenchloride; sulfur; In tetrahydrofuran; benzene;