CH₂CHCH₂CH₂C(CH₃)CHCH₂CH₂NHTs

Base Information

Chemical Name:CH₂CHCH₂CH₂C(CH₃)CHCH₂CH₂NHTs
CAS No.:757960-30-8
Molecular Formula:C₁₆H₂₃NO₂S
Molecular Weight:293.43
Hs Code.:

CH<sub>2</sub>CHCH<sub>2</sub>CH<sub>2</sub>C(CH<sub>3</sub>)CHCH<sub>2</sub>CH<sub>2</sub>NHTs

Synonyms:CH₂CHCH₂CH₂C(CH₃)CHCH₂CH₂NHTs

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Chemical Property of CH₂CHCH₂CH₂C(CH₃)CHCH₂CH₂NHTs

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Technology Process of CH₂CHCH₂CH₂C(CH₃)CHCH₂CH₂NHTs

There total 3 articles about CH₂CHCH₂CH₂C(CH₃)CHCH₂CH₂NHTs which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 18522-92-4
sodium p-toluenesulfonamide

: 757960-33-1
8-iodo-5-methyl-1,5-octadiene

: 757960-30-8
(E)-CH₂CHCH₂CH₂C(CH₃)CHCH₂CH₂NHTs

Guidance literature:: In N,N-dimethyl-formamide; at 80 ℃; for 5h;
DOI:10.1016/j.tet.2004.06.023

Reference yield:

: 757960-32-0
5-(3-butenyl)-2,3-dihydrofuran

: 757960-30-8
(E)-CH₂CHCH₂CH₂C(CH₃)CHCH₂CH₂NHTs

Guidance literature:: Multi-step reaction with 4 steps

1: 79 percent / (Ph₃P)2NiCl₂ / toluene / 1.5 h / 80 °C

2: Et₃N / CH₂Cl₂

3: NaI / acetone

4: 72 percent / dimethylformamide / 5 h / 80 °C

With triethylamine; sodium iodide; bis(triphenylphosphine)nickel(II) chloride; In dichloromethane; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/j.tet.2004.06.023

Reference yield:

: Methanesulfonic acid (E)-4-methyl-octa-3,7-dienyl ester

: 757960-30-8
(E)-CH₂CHCH₂CH₂C(CH₃)CHCH₂CH₂NHTs

Guidance literature:: Multi-step reaction with 2 steps

1: NaI / acetone

2: 72 percent / dimethylformamide / 5 h / 80 °C

With sodium iodide; In N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.tet.2004.06.023