2-<1-<2-Hydroxy-4-(3,4,5,6-tetrahydr-2H-thiopyran-3-yl)-6-oxo-1-cyclohexen-1-yl>cyclopropyl>essigsaeure-ethylester

Base Information

Chemical Name:2-<1-<2-Hydroxy-4-(3,4,5,6-tetrahydr-2H-thiopyran-3-yl)-6-oxo-1-cyclohexen-1-yl>cyclopropyl>essigsaeure-ethylester
CAS No.:120229-78-9
Molecular Formula:C₁₈H₂₆O₄S
Molecular Weight:338.468
Hs Code.:

Synonyms:2-<1-<2-Hydroxy-4-(3,4,5,6-tetrahydr-2H-thiopyran-3-yl)-6-oxo-1-cyclohexen-1-yl>cyclopropyl>essigsaeure-ethylester

Suppliers and Price of 2-<1-<2-Hydroxy-4-(3,4,5,6-tetrahydr-2H-thiopyran-3-yl)-6-oxo-1-cyclohexen-1-yl>cyclopropyl>essigsaeure-ethylester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-<1-<2-Hydroxy-4-(3,4,5,6-tetrahydr-2H-thiopyran-3-yl)-6-oxo-1-cyclohexen-1-yl>cyclopropyl>essigsaeure-ethylester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-<1-<2-Hydroxy-4-(3,4,5,6-tetrahydr-2H-thiopyran-3-yl)-6-oxo-1-cyclohexen-1-yl>cyclopropyl>essigsaeure-ethylester

There total 3 articles about 2-<1-<2-Hydroxy-4-(3,4,5,6-tetrahydr-2H-thiopyran-3-yl)-6-oxo-1-cyclohexen-1-yl>cyclopropyl>essigsaeure-ethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 120229-76-7
2-Ethoxy-5,6,7,8-tetrahydro-7-(3,4,5,6-tetrahydro-2H-thiopyran-3-yl)spiro<4H-chromen-4,1'-cyclopropan>-5-on

: 120229-78-9
2-<1-<2-Hydroxy-4-(3,4,5,6-tetrahydr-2H-thiopyran-3-yl)-6-oxo-1-cyclohexen-1-yl>cyclopropyl>essigsaeure-ethylester

Guidance literature:: With sodium hydrogen sulfate; In dichloromethane; at 40 ℃; for 24h;

Reference yield:

: 120229-87-0
3-hydroxy-5-(tetrahydro-2H-thiopyran-3-yl)-2-cyclohexen-1-one

: 120229-78-9
2-<1-<2-Hydroxy-4-(3,4,5,6-tetrahydr-2H-thiopyran-3-yl)-6-oxo-1-cyclohexen-1-yl>cyclopropyl>essigsaeure-ethylester

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / acetonitrile / 24 h / 20 °C

2: 1) ethyldisopropylamine, 2) acetylchloride / 1) CH₂Cl₂, 0 deg C, 10 min, 2) 16 h, reflux

3: 74 percent / 1M NaHSO₄ aq. / CH₂Cl₂ / 24 h / 40 °C

With sodium hydrogen sulfate; N-ethyl-N,N-diisopropylamine; acetyl chloride; In dichloromethane; acetonitrile;

Reference yield:

: 120229-75-6
3-Hydroxy-2-(1-piperidinocyclopropyl)-5-(3,4,5,6-tetrahydro-2H-thiopyran-3-yl)-2-cyclohexen-1-on

: 120229-78-9
2-<1-<2-Hydroxy-4-(3,4,5,6-tetrahydr-2H-thiopyran-3-yl)-6-oxo-1-cyclohexen-1-yl>cyclopropyl>essigsaeure-ethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) ethyldisopropylamine, 2) acetylchloride / 1) CH₂Cl₂, 0 deg C, 10 min, 2) 16 h, reflux

2: 74 percent / 1M NaHSO₄ aq. / CH₂Cl₂ / 24 h / 40 °C

With sodium hydrogen sulfate; N-ethyl-N,N-diisopropylamine; acetyl chloride; In dichloromethane;