3-(((S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)-1-(((S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)piperidine

Base Information

Chemical Name:3-(((S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)-1-(((S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)piperidine
CAS No.:1426690-22-3
Molecular Formula:C₂₅H₃₉N
Molecular Weight:353.591
Hs Code.:

Synonyms:3-(((S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)-1-(((S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)piperidine

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Chemical Property of 3-(((S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)-1-(((S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)piperidine

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Technology Process of 3-(((S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)-1-(((S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)piperidine

There total 3 articles about 3-(((S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)-1-(((S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 18031-40-8
(S)-(-)-perillaldehyde

: 1426690-10-9
(S)-1-((4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)piperidine

: 1426690-22-3
3-(((S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)-1-(((S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)piperidine

Guidance literature:: (S)-(-)-perillaldehyde; (S)-1-((4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)piperidine; With [Ru(p-cymene)(k⁽²⁾-o-tBuPPBS)Cl]; (1S)-10-camphorsulfonic acid; In toluene; at 150 ℃; for 16h; Schlenk technique;

With formic acid; In toluene; at 130 ℃; for 3h; Schlenk technique;
DOI:10.1039/c3gc36982j

Reference yield:

: 110-89-4
piperidine

: 1426690-22-3
3-(((S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)-1-(((S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)piperidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: formic acid / neat (no solvent) / 16 h / 100 °C / Schlenk technique

2.1: (1S)-10-camphorsulfonic acid; [Ru(p-cymene)(k⁽²⁾-o-tBuPPBS)Cl] / toluene / 16 h / 150 °C / Schlenk technique

2.2: 3 h / 130 °C / Schlenk technique

With formic acid; [Ru(p-cymene)(k⁽²⁾-o-tBuPPBS)Cl]; (1S)-10-camphorsulfonic acid; In toluene; 1.1: |Leukardt-Wallach Amination;
DOI:10.1039/c3gc36982j

Reference yield:

: 18031-40-8
(S)-(-)-perillaldehyde

: 1426690-22-3
3-(((S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)-1-(((S)-4-(prop-1-en-2-yl)cyclohex-1-en-1-yl)methyl)piperidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: formic acid / neat (no solvent) / 16 h / 100 °C / Schlenk technique

2.1: (1S)-10-camphorsulfonic acid; [Ru(p-cymene)(k⁽²⁾-o-tBuPPBS)Cl] / toluene / 16 h / 150 °C / Schlenk technique

2.2: 3 h / 130 °C / Schlenk technique

With formic acid; [Ru(p-cymene)(k⁽²⁾-o-tBuPPBS)Cl]; (1S)-10-camphorsulfonic acid; In toluene; 1.1: |Leukardt-Wallach Amination;
DOI:10.1039/c3gc36982j