C₆₆H₇₆N₂O₁₁

Base Information

Chemical Name:C₆₆H₇₆N₂O₁₁
CAS No.:848827-43-0
Molecular Formula:C₆₆H₇₆N₂O₁₁
Molecular Weight:1073.34
Hs Code.:

C<sub>66</sub>H<sub>76</sub>N<sub>2</sub>O<sub>11</sub>

Synonyms:C₆₆H₇₆N₂O₁₁

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Chemical Property of C₆₆H₇₆N₂O₁₁

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Technology Process of C₆₆H₇₆N₂O₁₁

There total 5 articles about C₆₆H₇₆N₂O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 848827-42-9
C₅₂H₄₇NO₁₂

: 2016-42-4
tetradecylamine

: 848827-43-0
C₆₆H₇₆N₂O₁₁

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1-hydroxybenzotriazol-hydrate; In 1,2-dichloro-ethane;
DOI:10.1016/j.tet.2004.12.027

Reference yield:

: C₃₄H₃₂O₈

: 848827-43-0
C₆₆H₇₆N₂O₁₁

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / 1H-tetrazole / tetrahydrofuran / 2 h / 20 °C

2: 95 percent / trifluoromethanesulfonic acid; molecular sieves 4 Angstroem / CH₂Cl₂ / 1 h / 20 °C

3: 92 percent / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / tetrahydrofuran

4: 100 percent / 1-hydroxybenzotriazole hydrate; HBTU / 1,2-dichloro-ethane

With 1H-tetrazole; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trifluorormethanesulfonic acid; 4 A molecular sieve; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1-hydroxybenzotriazol-hydrate; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1016/j.tet.2004.12.027

Reference yield:

: C₄₁H₃₈O₇S

: 848827-43-0
C₆₆H₇₆N₂O₁₁

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / N-bromosuccinimide / acetone; H₂O / 2 h / 20 °C

2: 85 percent / 1H-tetrazole / tetrahydrofuran / 2 h / 20 °C

3: 95 percent / trifluoromethanesulfonic acid; molecular sieves 4 Angstroem / CH₂Cl₂ / 1 h / 20 °C

4: 92 percent / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / tetrahydrofuran

5: 100 percent / 1-hydroxybenzotriazole hydrate; HBTU / 1,2-dichloro-ethane

With 1H-tetrazole; N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; trifluorormethanesulfonic acid; 4 A molecular sieve; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1-hydroxybenzotriazol-hydrate; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; acetone;
DOI:10.1016/j.tet.2004.12.027