Technology Process of C36H55N3O10Si2
There total 5 articles about C36H55N3O10Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C23H40N2O8Si2;
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 20 ℃;
for 0.75h;
Inert atmosphere;
O-Benzyl-D-serine allyl ester;
In
dichloromethane;
at 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/jo202061t
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: water; lithium hydroxide / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere
1.2: Amberlyst-15 / pH 5 / Inert atmosphere
2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.75 h / 20 °C / Inert atmosphere
2.2: 2 h / 20 °C / Inert atmosphere
With
water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium hydroxide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/jo202061t
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / water; acetonitrile / 0.67 h / 25 °C / Inert atmosphere
2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.75 h / 20 °C / Inert atmosphere
2.2: 2 h / 20 °C / Inert atmosphere
With
2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane; water; acetonitrile;
DOI:10.1021/jo202061t
