2-(6-chlorobenzo[pqr]tetraphen-1-yl)cyclohexanol

Base Information

Chemical Name:2-(6-chlorobenzo[pqr]tetraphen-1-yl)cyclohexanol
CAS No.:111189-45-8
Molecular Formula:C₂₆H₂₁ClO
Molecular Weight:384.905
Hs Code.:

Synonyms:2-(6-chloro-1-benzopyrenyl)cyclohexanol

Suppliers and Price of 2-(6-chlorobenzo[pqr]tetraphen-1-yl)cyclohexanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(6-chlorobenzo[pqr]tetraphen-1-yl)cyclohexanol

Chemical Property:

Vapor Pressure:5.12E-16mmHg at 25°C

Purity/Quality:

Safty Information:

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Technology Process of 2-(6-chlorobenzo[pqr]tetraphen-1-yl)cyclohexanol

There total 1 articles about 2-(6-chlorobenzo[pqr]tetraphen-1-yl)cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21248-01-1
6-Chlorobenzo[a]pyrene

: 286-20-4
cyclohexane-1,2-epoxide

: 111189-56-1
2-(6-Chloro-benzo[def]chrysen-3-yl)-cyclohexanol

: 111189-45-8
2-(6-chloro-1-benzo pyrenyl)cyclohexanol

Guidance literature:: Yield given. Multistep reaction. Yields of byproduct given;
DOI:10.1021/jo00235a005

Reference yield: 71.0%

: 111189-45-8
2-(6-chloro-1-benzo pyrenyl)cyclohexanol

: 111189-46-9
2-(6-Chloro-benzo[def]chrysen-1-yl)-cyclohexanone

Guidance literature:: With Dess-Martin periodane; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1021/jo00235a005

Reference yield:

: 111189-45-8
2-(6-chloro-1-benzo pyrenyl)cyclohexanol

: 111189-34-5
Benzindeno<1,2,3qr>chrysene

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / Dess-Martin reagent / CH₂Cl₂ / 2 h / Ambient temperature

2: 1.) polyphosphoric acid (PPA), 2.) 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) / 1.) 150 deg C, 5 h, 2.) benzene, reflux, 10 min

With PPA; Dess-Martin periodane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane;
DOI:10.1021/jo00235a005