(E)-1-(4-chlorophenyl)-3-(2,3,5,6-tetrafluoro-4-methoxyphenyl)prop-1-ene

Base Information

Chemical Name:(E)-1-(4-chlorophenyl)-3-(2,3,5,6-tetrafluoro-4-methoxyphenyl)prop-1-ene
CAS No.:1616842-56-8
Molecular Formula:C₁₆H₁₁ClF₄O
Molecular Weight:330.709
Hs Code.:

Synonyms:(E)-1-(4-chlorophenyl)-3-(2,3,5,6-tetrafluoro-4-methoxyphenyl)prop-1-ene

Suppliers and Price of (E)-1-(4-chlorophenyl)-3-(2,3,5,6-tetrafluoro-4-methoxyphenyl)prop-1-ene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-(4-chlorophenyl)-3-(2,3,5,6-tetrafluoro-4-methoxyphenyl)prop-1-ene

Chemical Property:

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Technology Process of (E)-1-(4-chlorophenyl)-3-(2,3,5,6-tetrafluoro-4-methoxyphenyl)prop-1-ene

There total 7 articles about (E)-1-(4-chlorophenyl)-3-(2,3,5,6-tetrafluoro-4-methoxyphenyl)prop-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24393-52-0
ethyl (E)-3-(4-chlorophenyl)prop-2-enoate

: 1616842-56-8
(E)-1-(4-chlorophenyl)-3-(2,3,5,6-tetrafluoro-4-methoxyphenyl)prop-1-ene

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / toluene / 1 h / -78 °C / Inert atmosphere

2: phosphorus tribromide / diethyl ether / 1 h / 0 °C / Inert atmosphere

3: Triphenylphosphine oxide / hexane; tetrahydrofuran / 16 h / 75 °C / Schlenk technique; Inert atmosphere

With phosphorus tribromide; diisobutylaluminium hydride; Triphenylphosphine oxide; In tetrahydrofuran; diethyl ether; hexane; toluene;
DOI:10.1016/j.tet.2015.05.107

Reference yield:

: C₈H₆F₄OZn

: 42432-30-4,60691-90-9
p-chlorocinnamyl bromide

: 1616842-56-8
(E)-1-(4-chlorophenyl)-3-(2,3,5,6-tetrafluoro-4-methoxyphenyl)prop-1-ene

Guidance literature:: With Triphenylphosphine oxide; In tetrahydrofuran; hexane; at 75 ℃; for 16h; chemoselective reaction; Schlenk technique; Inert atmosphere;
DOI:10.1016/j.tet.2015.05.107

Reference yield:

: 24583-70-8
(E)-3-(p-chlorophenyl)prop-2-en-1-ol

: 1616842-56-8
(E)-1-(4-chlorophenyl)-3-(2,3,5,6-tetrafluoro-4-methoxyphenyl)prop-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus tribromide / diethyl ether / 1 h / 0 °C / Inert atmosphere

2: Triphenylphosphine oxide / hexane; tetrahydrofuran / 16 h / 75 °C / Schlenk technique; Inert atmosphere

With phosphorus tribromide; Triphenylphosphine oxide; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1016/j.tet.2015.05.107