1-<(4-chloro-3-sulfamoylphenyl)sulfonyl>-4-(ethoxycarbonyl)piperazine

Base Information

Chemical Name:1-<(4-chloro-3-sulfamoylphenyl)sulfonyl>-4-(ethoxycarbonyl)piperazine
CAS No.:145389-79-3
Molecular Formula:C₁₃H₁₈ClN₃O₆S₂
Molecular Weight:411.887
Hs Code.:

Synonyms:1-<(4-chloro-3-sulfamoylphenyl)sulfonyl>-4-(ethoxycarbonyl)piperazine

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Chemical Property of 1-<(4-chloro-3-sulfamoylphenyl)sulfonyl>-4-(ethoxycarbonyl)piperazine

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Technology Process of 1-<(4-chloro-3-sulfamoylphenyl)sulfonyl>-4-(ethoxycarbonyl)piperazine

There total 1 articles about 1-<(4-chloro-3-sulfamoylphenyl)sulfonyl>-4-(ethoxycarbonyl)piperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 120-43-4
4-ethoxycarbonylpiperazine

: 61450-06-4
4-chloro-3-sulfamoylbenzenesulfonyl chloride

: 145389-79-3
1-<(4-chloro-3-sulfamoylphenyl)sulfonyl>-4-(ethoxycarbonyl)piperazine

Guidance literature:: With triethylamine; In acetone; for 0.333333h; Ambient temperature;
DOI:10.1021/jm00053a020

Reference yield: 96.0%

: 145389-79-3
1-<(4-chloro-3-sulfamoylphenyl)sulfonyl>-4-(ethoxycarbonyl)piperazine

: 145389-80-6
1-<(4-chloro-3-sulfamoylphenyl)sulfonyl>piperazine

Guidance literature:: With sodium carbonate; In water; for 20h; Heating;
DOI:10.1021/jm00053a020

Reference yield:

: 145389-79-3
1-<(4-chloro-3-sulfamoylphenyl)sulfonyl>-4-(ethoxycarbonyl)piperazine

: 2-Chloro-5-{4-[2-hydroxy-3-(naphthalen-1-yloxy)-propyl]-piperazine-1-sulfonyl}-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / 10percent aq. Na₂CO₃ / H₂O / 20 h / Heating

2: 55 percent / ethanol / 12 h / Heating

With sodium carbonate; In ethanol; water;
DOI:10.1021/jm00053a020