[1-¹⁵N]-3-[(2-acetoxyethoxy)methyl]-6-phenyl-1,2,4-triazolo[1,5-a]pyrimidin-7-one

Base Information

• Chemical Name: [1-¹⁵N]-3-[(2-acetoxyethoxy)methyl]-6-phenyl-1,2,4-triazolo[1,5-a]pyrimidin-7-one
• CAS No.: 1585165-22-5
• Molecular Formula: C₁₆H₁₆N₄O₄
• Molecular Weight: 329.321

Synonyms:[1-¹⁵N]-3-[(2-acetoxyethoxy)methyl]-6-phenyl-1,2,4-triazolo[1,5-a]pyrimidin-7-one

Chemical Property of [1-¹⁵N]-3-[(2-acetoxyethoxy)methyl]-6-phenyl-1,2,4-triazolo[1,5-a]pyrimidin-7-one

Chemical Property:

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Technology Process of [1-¹⁵N]-3-[(2-acetoxyethoxy)methyl]-6-phenyl-1,2,4-triazolo[1,5-a]pyrimidin-7-one

There total 4 articles about [1-¹⁵N]-3-[(2-acetoxyethoxy)methyl]-6-phenyl-1,2,4-triazolo[1,5-a]pyrimidin-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-[(2-acetoxyethoxy)methyl]-5-methyl-1,2,4-triazolo[1,5-a]pyrimidin-7-one (331723-29-6) + [1-15N]-6-phenyl-1,2,4-triazolo[1,5-a]pyrimidin-7-one (1542213-45-5) → [1-15N]-3-[(2-acetoxyethoxy)methyl]-6-phenyl-1,2,4-triazolo[1,5-a]pyrimidin-7-one (1585165-22-5) + [1-15N]-4-[(2-acetoxyethoxy)methyl]-6-phenyl-1,2,4-triazolo[1,5-a]pyrimidin-7-one (1585165-23-6)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 20 ℃; for 0.5h;

DOI:10.1016/j.tet.2013.12.051

Reference yield:

4-[(2-acetoxyethoxy)methyl]-6-phenyl-1,2,4-triazolo[1,5-a]pyrimidin-7-one (1542213-35-3) + [1-15N]-6-phenyl-1,2,4-triazolo[1,5-a]pyrimidin-7-one (1542213-45-5) → [1-15N]-3-[(2-acetoxyethoxy)methyl]-6-phenyl-1,2,4-triazolo[1,5-a]pyrimidin-7-one (1585165-22-5) + [1-15N]-4-[(2-acetoxyethoxy)methyl]-6-phenyl-1,2,4-triazolo[1,5-a]pyrimidin-7-one (1585165-23-6)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 20 ℃; for 720h;

DOI:10.1016/j.tet.2013.12.051

Reference yield:

2-acetoxyethyl acetoxymethyl ether (59278-00-1) → [1-15N]-3-[(2-acetoxyethoxy)methyl]-6-phenyl-1,2,4-triazolo[1,5-a]pyrimidin-7-one (1585165-22-5) + [1-15N]-4-[(2-acetoxyethoxy)methyl]-6-phenyl-1,2,4-triazolo[1,5-a]pyrimidin-7-one (1585165-23-6)

Guidance literature:

Multi-step reaction with 2 steps

1: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 0.2 h / 20 °C

2: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 0.5 h / 20 °C

With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; 1: |Vorbrueggen Nucleoside Synthesis;

DOI:10.1016/j.tet.2013.12.051

upstream raw materials:

3-[(2-acetoxyethoxy)methyl]-5-methyl-1,2,4-triazolo[1,5-a]pyrimidin-7-one

[1-¹⁵N]-6-phenyl-1,2,4-triazolo[1,5-a]pyrimidin-7-one

4-[(2-acetoxyethoxy)methyl]-6-phenyl-1,2,4-triazolo[1,5-a]pyrimidin-7-one

phenyl(formyl)acetonitrile

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