N-<5(S)-amino-4(S)-hydroxy-6-cyclohexyl-2(S)-isopropylhexanoyl>-2(S)-methylbutylamine hydrochloride

Base Information

Chemical Name:N-<5(S)-amino-4(S)-hydroxy-6-cyclohexyl-2(S)-isopropylhexanoyl>-2(S)-methylbutylamine hydrochloride
CAS No.:124322-07-2
Molecular Formula:C₂₀H₄₀N₂O₂*ClH
Molecular Weight:413.472
Hs Code.:

Synonyms:N-<5(S)-amino-4(S)-hydroxy-6-cyclohexyl-2(S)-isopropylhexanoyl>-2(S)-methylbutylamine hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<5(S)-amino-4(S)-hydroxy-6-cyclohexyl-2(S)-isopropylhexanoyl>-2(S)-methylbutylamine hydrochloride

Chemical Property:

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Technology Process of N-<5(S)-amino-4(S)-hydroxy-6-cyclohexyl-2(S)-isopropylhexanoyl>-2(S)-methylbutylamine hydrochloride

There total 4 articles about N-<5(S)-amino-4(S)-hydroxy-6-cyclohexyl-2(S)-isopropylhexanoyl>-2(S)-methylbutylamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124322-05-0
N-<4-(S)-<(tert-butyldimethylsilyl)oxy>-5(S)-<(tert-butyloxycarbonyl)amino>-6-cyclohexyl-2(S)-isopropylhexanoyl>-2(S)-methylbutylamine

: 124322-07-2
N-<5(S)-amino-4(S)-hydroxy-6-cyclohexyl-2(S)-isopropylhexanoyl>-2(S)-methylbutylamine hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; for 0.25h;
DOI:10.1021/jm00108a006

Reference yield:

: 124322-05-0
N-<4-(S)-<(tert-butyldimethylsilyl)oxy>-5(S)-<(tert-butyloxycarbonyl)amino>-6-cyclohexyl-2(S)-isopropylhexanoyl>-2(S)-methylbutylamine

: 124322-07-2
(2S,4S,5S)-5-Amino-6-cyclohexyl-4-hydroxy-2-isopropyl-hexanoic acid ((S)-2-methyl-butyl)-amide; hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; for 0.25h;
DOI:10.1021/jm00167a009

Reference yield:

: 34985-37-0
(S)-2-methylbutylamine

: 124322-07-2
N-<5(S)-amino-4(S)-hydroxy-6-cyclohexyl-2(S)-isopropylhexanoyl>-2(S)-methylbutylamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / diisopropylethylamine, diethylphosphoryl cyanide / CH₂Cl₂ / 3 h / 0 - 25 °C

2: 1.15 g / HCl(gas) / diethyl ether / 0.25 h

With hydrogenchloride; diethylphosphoryl cyanide; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane;
DOI:10.1021/jm00108a006