C₃₈H₄₂N₆O₁₃

Base Information

Chemical Name:C₃₈H₄₂N₆O₁₃
CAS No.:339087-23-9
Molecular Formula:C₃₈H₄₂N₆O₁₃
Molecular Weight:790.784
Hs Code.:

C<sub>38</sub>H<sub>42</sub>N<sub>6</sub>O<sub>13</sub>

Synonyms:C₃₈H₄₂N₆O₁₃

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Chemical Property of C₃₈H₄₂N₆O₁₃

Chemical Property:

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Technology Process of C₃₈H₄₂N₆O₁₃

There total 15 articles about C₃₈H₄₂N₆O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Boc-[(L)-Asp(OBzl)-(L)-Thr]OCH₂CCl₃

: 339087-23-9
C₃₈H₄₂N₆O₁₃

Guidance literature:: Multi-step reaction with 9 steps

1: DAST / CH₂Cl₂ / 2 h / -78 °C

2: 23 percent / DBU; BrCCl₃ / CH₂Cl₂ / 0 - 20 °C

3: CH₂Cl₂ / 20 °C

4: 68 percent / HBTU; HOBt; DIEA / dimethylformamide / 96 h / -20 - 20 °C

5: CH₂Cl₂ / 20 °C

6: HBTU; HOBt; DIEA / dimethylformamide / 96 h / -20 - 20 °C

7: Zn powder / acetic acid; H₂O / 5 h / 20 °C

8: CH₂Cl₂ / 1 h / 20 °C

9: PyBOP; DIEA / dimethylformamide / 240 h / 20 °C

With Bromotrichloromethane; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 4,4'-diaminostilbene-2,2'-disulfonic acid; zinc; In dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(00)01173-X

Reference yield:

: 339086-87-2
(S)-2-((S)-3-Benzyloxycarbonyl-2-tert-butoxycarbonylamino-propionylamino)-3-oxo-butyric acid 2,2,2-trichloro-ethyl ester

: 339087-23-9
C₃₈H₄₂N₆O₁₃

Guidance literature:: Multi-step reaction with 8 steps

1: 46 percent / Ph₃P; I₂; TEA / CH₂Cl₂ / 0 - 20 °C

2: CH₂Cl₂ / 20 °C

3: 68 percent / HBTU; HOBt; DIEA / dimethylformamide / 96 h / -20 - 20 °C

4: CH₂Cl₂ / 20 °C

5: HBTU; HOBt; DIEA / dimethylformamide / 96 h / -20 - 20 °C

6: Zn powder / acetic acid; H₂O / 5 h / 20 °C

7: CH₂Cl₂ / 1 h / 20 °C

8: PyBOP; DIEA / dimethylformamide / 240 h / 20 °C

With TEA; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; iodine; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; zinc; In dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(00)01173-X

Reference yield:

: 339086-88-3
2-(2-benzyloxycarbonyl-1-tert-butoxycarbonylamino-ethyl)-5-methyl-oxazole-4-carboxylic acid 2,2,2-trichloro-ethyl ester

: 339087-23-9
C₃₈H₄₂N₆O₁₃

Guidance literature:: Multi-step reaction with 7 steps

1: CH₂Cl₂ / 20 °C

2: 68 percent / HBTU; HOBt; DIEA / dimethylformamide / 96 h / -20 - 20 °C

3: CH₂Cl₂ / 20 °C

4: HBTU; HOBt; DIEA / dimethylformamide / 96 h / -20 - 20 °C

5: Zn powder / acetic acid; H₂O / 5 h / 20 °C

6: CH₂Cl₂ / 1 h / 20 °C

7: PyBOP; DIEA / dimethylformamide / 240 h / 20 °C

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; zinc; In dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(00)01173-X