C₃₀H₃₈O₇

Base Information

• Chemical Name: C₃₀H₃₈O₇
• CAS No.: 1262222-72-9
• Molecular Formula: C₃₀H₃₈O₇
• Molecular Weight: 510.628
• Mol file: 1262222-72-9.mol

Synonyms:C₃₀H₃₈O₇

Chemical Property of C₃₀H₃₈O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₃₈O₇

There total 1 articles about C₃₀H₃₈O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

3-methoxy-4-(phenylmethoxy)benzaldehyde (2426-87-1) + (3R,2'S)-(1',4'-dioxa-spiro[4.5]dec-2'-yl)-pent-4-enoic acid ethyl ester (727428-95-7) → C30H38O7 + C30H38O7 (1262222-72-9)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 4h;

DOI:10.1016/j.tetlet.2010.10.136

Reference yield: 70.0%

C30H38O7 (1262222-72-9) → C23H26O6

Guidance literature:

With sodium periodate; acetic acid; In water; at 20 ℃; for 16h;

DOI:10.1016/j.tetlet.2010.10.136

Reference yield:

C30H38O7 (1262222-72-9) → C21H26O4 (1262222-76-3)

Guidance literature:

Multi-step reaction with 8 steps

1: sodium periodate; acetic acid / water / 16 h / 20 °C

2: hydrogenchloride / 4 h / 20 °C

3: sodium periodate; osmium(VIII) oxide / tetrahydrofuran; water / 6 h / 0 - 20 °C

4: sodium tetrahydroborate / methanol / 1 h / 0 °C

5: silica gel

6: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C

7: triethylamine / dichloromethane / 2 h / 0 °C

8: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 20 °C

With hydrogenchloride; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; lithium aluminium tetrahydride; silica gel; acetic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water;

DOI:10.1016/j.tetlet.2010.10.136

upstream raw materials:

3-methoxy-4-(phenylmethoxy)benzaldehyde

(3R,2'S)-(1',4'-dioxa-spiro[4.5]dec-2'-yl)-pent-4-enoic acid ethyl ester

Downstream raw materials:

C₂₁H₂₆O₄

C₂₀H₂₂O₄

C₂₁H₂₆O₅

C₂₄H₂₈O₆