3-(p-tolyl)-1,4-dihydro-1,7-dimethyl-6-oxo-4H-<1,2,4>triazino<4,3-b><1,2,4,5>tetrazine

Base Information

Chemical Name:3-(p-tolyl)-1,4-dihydro-1,7-dimethyl-6-oxo-4H-<1,2,4>triazino<4,3-b><1,2,4,5>tetrazine
CAS No.:116471-38-6
Molecular Formula:C₁₃H₁₄N₆O
Molecular Weight:270.294
Hs Code.:

Synonyms:3-(p-tolyl)-1,4-dihydro-1,7-dimethyl-6-oxo-4H-<1,2,4>triazino<4,3-b><1,2,4,5>tetrazine

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Chemical Property of 3-(p-tolyl)-1,4-dihydro-1,7-dimethyl-6-oxo-4H-<1,2,4>triazino<4,3-b><1,2,4,5>tetrazine

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Technology Process of 3-(p-tolyl)-1,4-dihydro-1,7-dimethyl-6-oxo-4H-<1,2,4>triazino<4,3-b><1,2,4,5>tetrazine

There total 4 articles about 3-(p-tolyl)-1,4-dihydro-1,7-dimethyl-6-oxo-4H-<1,2,4>triazino<4,3-b><1,2,4,5>tetrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 116471-27-3
3-(p-tolyl)-1,2,3,4-tetrahydro-1,7-dimethyl-6-oxo-2H,4H-<1,2,4>triazino<4,3-b><1,2,4,5>tetrazine

: 116471-38-6
3-(p-tolyl)-1,4-dihydro-1,7-dimethyl-6-oxo-4H-<1,2,4>triazino<4,3-b><1,2,4,5>tetrazine

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene; for 4h; Heating;
DOI:10.1016/S0040-4020(01)81733-6

Reference yield: 53.0%

: 116471-24-0
6-methyl-3-(1-methylhydrazino)-5-oxo-4-thriphenylphosphoranylideneamino-4,5-dihydro<1,2,4>triazine

: 874-60-2
4-methyl-benzoyl chloride

: 116471-38-6
3-(p-tolyl)-1,4-dihydro-1,7-dimethyl-6-oxo-4H-<1,2,4>triazino<4,3-b><1,2,4,5>tetrazine

Guidance literature:: With triethylamine; In benzene; for 6h; Heating;
DOI:10.1016/S0040-4020(01)81733-6

Reference yield:

: 116471-23-9
4-amino-6-methyl-3-(1-methylhydrazino)-5-oxo-4,5-dihydro<1,2,4>triazine

: 116471-38-6
3-(p-tolyl)-1,4-dihydro-1,7-dimethyl-6-oxo-4H-<1,2,4>triazino<4,3-b><1,2,4,5>tetrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / 1N HCl / ethanol / 6 h / Heating

2: 93 percent / 2,3-dichloro-5,6-dicyanobenzoquinone / benzene / 4 h / Heating

With hydrogenchloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In ethanol; benzene;
DOI:10.1016/S0040-4020(01)81733-6