Benzyl-3-O--2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

Base Information

Chemical Name:Benzyl-3-O--2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid
CAS No.:92075-31-5
Molecular Formula:C₂₉H₃₇NO₁₄*H₃N
Molecular Weight:640.642
Hs Code.:

Benzyl-3-O-<ammonium-(3-desoxy-α-D-manno-2-octulopyranosyl)onat>-2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

Synonyms:Benzyl-3-O--2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl-3-O--2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

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Technology Process of Benzyl-3-O--2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

There total 6 articles about Benzyl-3-O--2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 92052-01-2
Benzyl-4,6-di-O-acetyl-2-(benzyloxycarbonyl)amino-2-desoxy-3-O-<(4,5,7,8-tetra-O-acetyl-3-desoxy-α-D-manno-2-octulopyranosyl)onsaeure>-α-D-glucopyranosid

: 92075-31-5
Benzyl-3-O--2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

Guidance literature:: With ammonium hydroxide; sodium hydroxide; Dowex 5O W; hydrogen cation; In methanol; for 18h;

Reference yield:

: 85382-91-8,85382-92-9
Benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-4,6-O-ethyliden-3-O--α-D-glucopyranosid

: 92075-31-5
Benzyl-3-O--2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

Guidance literature:: With ammonium hydroxide; sodium hydroxide; Dowex 50 W; hydrogen cation; trifluoroacetic acid; Yield given. Multistep reaction; 1.) methylene dichloride, 5 h, 2.) methanol, 1.5 h;

Reference yield:

: 148152-74-3
methyl (4,5,7,8-tetra-O-acetyl-3-deoxy-α-D-manno-2-octulopyranosyl bromide)onate

: 92075-31-5
Benzyl-3-O--2-(benzyloxycarbonyl)amino-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 43 percent / HgCN₂/HgBr₂/molecular sieve (4 Angstroem) / CH₂Cl₂; toluene / 20 °C

2: 1.) 90percent CF₃COOH, 2.) pyridine/4-(dimethylamino)pyridine / 1.) methylene dichloride, 5 h, 2.) methylene dichloride, 0 deg C, 18 h

3: 84 percent / 0.5 N NaOH; Dowex 5O W, H⁽¹⁺⁾-form; conc. NH₃ / methanol / 18 h

With pyridine; dmap; ammonium hydroxide; sodium hydroxide; 4 A molecular sieve; Dowex 5O W; mercury(II) cyanide; hydrogen cation; trifluoroacetic acid; mercury dibromide; In methanol; dichloromethane; toluene;