2-(2,4-dinitrophenyl)ethyl vinyl ether

Base Information

Chemical Name:2-(2,4-dinitrophenyl)ethyl vinyl ether
CAS No.:213548-15-3
Molecular Formula:C₁₀H₁₀N₂O₅
Molecular Weight:238.2
Hs Code.:

Synonyms:2-(2,4-dinitrophenyl)ethyl vinyl ether

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Chemical Property of 2-(2,4-dinitrophenyl)ethyl vinyl ether

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Technology Process of 2-(2,4-dinitrophenyl)ethyl vinyl ether

There total 1 articles about 2-(2,4-dinitrophenyl)ethyl vinyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 4836-69-5
β-(2,4-dinitrophenyl)ethyl alcohol

: 109-92-2,25104-37-4
ethyl vinyl ether

: 213548-15-3
2-(2,4-dinitrophenyl)ethyl vinyl ether

Guidance literature:: With mercury(II) trifluoroacetate; for 1h; Ambient temperature;
DOI:10.1002/hlca.19980810557

Reference yield: 86.0%

: 213548-15-3
2-(2,4-dinitrophenyl)ethyl vinyl ether

: 69304-38-7
3',5'-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

: 213548-56-2
2'-O-{1-[2-(2,4-dinitrophenyl)ethoxy]ethyl}-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)uridine

Guidance literature:: With toluene-4-sulfonic acid; In toluene; at 20 ℃; for 6h;
DOI:10.1002/hlca.19980810557

Reference yield:

: 213548-15-3
2-(2,4-dinitrophenyl)ethyl vinyl ether

: 2'-O-{1-[2-(2,4-dinitrophenyl)ethoxy]ethyl}uridine

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / TsOH / toluene / 6 h / 20 °C

2: 76 percent / 0.16M Bu₃NF*3H₂O, AcOH / dioxane / Ambient temperature

With Bu₃NF*3H₂O; toluene-4-sulfonic acid; acetic acid; In 1,4-dioxane; toluene;
DOI:10.1002/hlca.19980810557