N-(4-hydroxy-3-biphenyl)-2-methoxydibenzofuran-3-carboxamide

Base Information

• Chemical Name: N-(4-hydroxy-3-biphenyl)-2-methoxydibenzofuran-3-carboxamide
• CAS No.: 173312-46-4
• Molecular Formula: C₂₆H₁₉NO₄
• Molecular Weight: 409.441
• Mol file: 173312-46-4.mol

Synonyms:N-(4-hydroxy-3-biphenyl)-2-methoxydibenzofuran-3-carboxamide

Chemical Property of N-(4-hydroxy-3-biphenyl)-2-methoxydibenzofuran-3-carboxamide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of N-(4-hydroxy-3-biphenyl)-2-methoxydibenzofuran-3-carboxamide

There total 1 articles about N-(4-hydroxy-3-biphenyl)-2-methoxydibenzofuran-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-4-phenylphenol (1134-36-7) + 2-Methoxy-dibenzofuran-3-carbonyl chloride (1026900-67-3) → N-(4-hydroxy-3-biphenyl)-2-methoxydibenzofuran-3-carboxamide (173312-46-4)

Guidance literature:

With pyridine; In tetrahydrofuran; for 1h; Yield given;

DOI:10.1002/jhet.5570320523

Reference yield: 64.0%

N-(4-hydroxy-3-biphenyl)-2-methoxydibenzofuran-3-carboxamide (173312-46-4) → 2-methoxy-3-(5-phenyl-2-benzoxazolyl)dibenzofuran (173312-47-5)

Guidance literature:

With boric acid; In various solvent(s); at 255 - 260 ℃; for 0.5h;

DOI:10.1002/jhet.5570320523

Reference yield:

N-(4-hydroxy-3-biphenyl)-2-methoxydibenzofuran-3-carboxamide (173312-46-4) → 2-hydroxy-3-(5-phenyl-2-benzoxazolyl)dibenzofuran

Guidance literature:

Multi-step reaction with 2 steps

1: 64 percent / boric acid / various solvent(s) / 0.5 h / 255 - 260 °C

2: 94 percent / LiI, collidine / 1 h / Heating

With 2,3,5-trimethyl-pyridine; boric acid; lithium iodide; In various solvent(s);

DOI:10.1002/jhet.5570320523

upstream raw materials:

2-amino-4-phenylphenol

2-Methoxy-dibenzofuran-3-carbonyl chloride

Downstream raw materials:

2-methoxy-3-(5-phenyl-2-benzoxazolyl)dibenzofuran