Bicyclo[2.2.1]heptan-2-amine, 1,3,3-trimethyl-

Base Information

• Chemical Name: Bicyclo[2.2.1]heptan-2-amine, 1,3,3-trimethyl-
• CAS No.: 21252-46-0
• Molecular Formula: C10 H19 N
• Molecular Weight: 153.268
• Hs Code.: 2921300090
• Mol file: 21252-46-0.mol

Synonyms:2-Norbornanamine, 1,3,3-trimethyl- (6CI,7CI,8CI);1,3,3-Trimethylbicyclo[2.2.1]heptan-2-amine;

Chemical Property of Bicyclo[2.2.1]heptan-2-amine, 1,3,3-trimethyl-

Chemical Property:

• PSA: 26.02000
• LogP: 2.86020

Purity/Quality:

97% ^*data from raw suppliers

(1,3,3-trimethylbicyclo[2.2.1]hept-2-yl)amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Bicyclo[2.2.1]heptan-2-amine, 1,3,3-trimethyl-

There total 3 articles about Bicyclo[2.2.1]heptan-2-amine, 1,3,3-trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+/-)-fenchone (18492-37-0,126-21-6) + formamide (77287-34-4,77287-35-5,60100-09-6) → 1,3,3-trimethylbicyclo<2.2.1>heptan-2-endo-amine (4895-45-8,5003-94-1,21252-46-0,131348-01-1,131348-06-6,131348-10-2,131348-11-3,770696-39-4)

Guidance literature:

With formic acid; at 185 ℃; und Erwaermen einer Loesung des danach isolierten Reaktionsprodukts in Benzol mit wss.Salzsaeure;

DOI:10.1021/ja01300a089 DOI:10.1021/ja01151a109

Reference yield:

(+/-)-N-(1,3,3-trimethyl-[2endo]norbornyl)-formamide (6622-69-1,131348-00-0,131348-04-4,131348-08-8,131348-09-9) → 1,3,3-trimethylbicyclo<2.2.1>heptan-2-endo-amine (4895-45-8,5003-94-1,21252-46-0,131348-01-1,131348-06-6,131348-10-2,131348-11-3,770696-39-4)

Guidance literature:

(acid hydrolysis);

DOI:10.1021/jm01239a001

Reference yield:

→ 1,3,3-trimethylbicyclo[2.2.1]heptan-2-amine (21252-46-0,770696-39-4)

Guidance literature:

upstream raw materials:

(+/-)-fenchone

formamide

(+/-)-N-(1,3,3-trimethyl-[2endo]norbornyl)-formamide

Downstream raw materials:

limonene.

N-(1,3,3-trimethylbicyclo[2.2.1]hept-2-yl)-2-benzyl-3-(4-chloro-3-methylphenyl)-1,1-dioxo-1,2-dihydro-1^λ6-1,2,6-thiadiazine-5-carboxamide

N-(1,3,3-trimethylbicyclo[2.2.1]hept-2-yl)-2-benzyl-3-(4-chlorophenyl)-1,1-dioxo-1,2-dihydro-1^λ6-1,2,6-thiadiazine-5-carboxamide

N-(1,3,3-trimethylbicyclo[2.2.1]hept-2-yl)-2-(2,4-dichlorobenzyl)-3-(4-chlorophenyl)-1,1-dioxo-1,2-dihydro-1^λ6-1,2,6-thiadiazine-5-carboxamide

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