Technology Process of 2-(1E,3-butadienyl)phen-1-yl 2Z-butenoate
There total 3 articles about 2-(1E,3-butadienyl)phen-1-yl 2Z-butenoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate; hydrogen; ethylenediamine;
nickel diacetate;
In
ethanol;
at 20 ℃;
for 2.5h;
DOI:10.1021/jo0607818
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 75 percent / n-BuLi / tetrahydrofuran; hexane / 4 h / -18 - 20 °C
2: 97 percent / N,N'-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH2Cl2; diethyl ether / 5 h / 20 °C
3: 30 percent / hydrogen; NaBH4; ethylene diamine / nickel acetate tetrahydrate / ethanol / 2.5 h / 20 °C
With
dmap; sodium tetrahydroborate; n-butyllithium; hydrogen; ethylenediamine; dicyclohexyl-carbodiimide;
nickel diacetate;
In
tetrahydrofuran; diethyl ether; ethanol; hexane; dichloromethane;
DOI:10.1021/jo0607818
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 97 percent / N,N'-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH2Cl2; diethyl ether / 5 h / 20 °C
2: 30 percent / hydrogen; NaBH4; ethylene diamine / nickel acetate tetrahydrate / ethanol / 2.5 h / 20 °C
With
dmap; sodium tetrahydroborate; hydrogen; ethylenediamine; dicyclohexyl-carbodiimide;
nickel diacetate;
In
diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jo0607818
