[Cu(triphenylphosphine)2(2-phenyl-5-(pyridin-2-yl)-1,3,4-oxadiazole)]BF₄

Base Information

Chemical Name:[Cu(triphenylphosphine)2(2-phenyl-5-(pyridin-2-yl)-1,3,4-oxadiazole)]BF₄
CAS No.:1245722-49-9
Molecular Formula:BF₄*C₄₉H₃₉CuN₃OP₂
Molecular Weight:898.166
Hs Code.:

[Cu(triphenylphosphine)2(2-phenyl-5-(pyridin-2-yl)-1,3,4-oxadiazole)]BF<sub>4</sub>

Synonyms:[Cu(triphenylphosphine)2(2-phenyl-5-(pyridin-2-yl)-1,3,4-oxadiazole)]BF₄

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Chemical Property of [Cu(triphenylphosphine)2(2-phenyl-5-(pyridin-2-yl)-1,3,4-oxadiazole)]BF₄

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Technology Process of [Cu(triphenylphosphine)2(2-phenyl-5-(pyridin-2-yl)-1,3,4-oxadiazole)]BF₄

There total 5 articles about [Cu(triphenylphosphine)2(2-phenyl-5-(pyridin-2-yl)-1,3,4-oxadiazole)]BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 25433-30-1
2-(4-dimethylamino-penyl)-5-(2-pyridinyl)-1,3,4-oxadiazole

: tetrakis(acetonitrile)copper(I)tetrafluoroborate

: 603-35-0
triphenylphosphine

: 1245722-49-9
[Cu(triphenylphosphine)2(2-phenyl-5-(pyridin-2-yl)-1,3,4-oxadiazole)]BF₄

Guidance literature:: In dichloromethane; Cu compd. and P compd. refluxed in CH2Cl2 for 30 min, ligand added (1:2:1 molar ratio), refluxed for 30 min; evapd., recrystd. (THF/ether), elem. anal.;
DOI:10.1016/j.ica.2010.04.041

Reference yield:

: 65-85-0,8013-63-6
benzoic acid

: 1245722-49-9
[Cu(triphenylphosphine)2(2-phenyl-5-(pyridin-2-yl)-1,3,4-oxadiazole)]BF₄

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 24 h / 20 °C

2: pyridine / 72 h / Reflux

3: dichloromethane / 1 h

With thionyl chloride; In pyridine; dichloromethane;
DOI:10.1016/j.ica.2013.02.020

Reference yield:

: 100-70-9,1232006-36-8
2-Cyanopyridine

: 1245722-49-9
[Cu(triphenylphosphine)2(2-phenyl-5-(pyridin-2-yl)-1,3,4-oxadiazole)]BF₄

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide; zinc dibromide / water / 6 h / Reflux

2: pyridine / 72 h / Reflux

3: dichloromethane / 1 h

With sodium azide; zinc dibromide; In pyridine; dichloromethane; water;
DOI:10.1016/j.ica.2013.02.020