Technology Process of C21H26N4O5S
There total 6 articles about C21H26N4O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C
2: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water / 0.5 h / 100 °C
3: lithium borohydride / tetrahydrofuran / 2 h / Reflux
With
potassium phosphate; lithium borohydride; n-butyllithium;
bis-triphenylphosphine-palladium(II) chloride;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / dichloromethane / 16 h / 20 °C
2.1: lithium diisopropyl amide / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere
2.2: 0 - 20 °C
3.1: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water / 0.5 h / 100 °C
4.1: lithium borohydride / tetrahydrofuran / 2 h / Reflux
With
potassium phosphate; lithium borohydride; potassium carbonate; lithium diisopropyl amide;
bis-triphenylphosphine-palladium(II) chloride;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere
1.2: 0 - 20 °C
2.1: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water / 0.5 h / 100 °C
3.1: lithium borohydride / tetrahydrofuran / 2 h / Reflux
With
potassium phosphate; lithium borohydride; lithium diisopropyl amide;
bis-triphenylphosphine-palladium(II) chloride;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;