Technology Process of 7-amino-3-(3-methoxyphenyl)-9H-carbazole-1-carboxamide
There total 9 articles about 7-amino-3-(3-methoxyphenyl)-9H-carbazole-1-carboxamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium formate;
palladium 10% on activated carbon;
In
methanol;
for 1h;
Inert atmosphere;
Reflux;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: sodium nitrite; hydrogenchloride; tin(ll) chloride
2: acetone / Reflux
3: 1,2-dichloro-ethane; benzotriazol-1-ol; ammonium hydroxide / tetrahydrofuran; dichloromethane
4: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / Reflux
5: sodium hydroxide; water / methanol; tetrahydrofuran
6: diphenyl phosphoryl azide; triethylamine
7: trifluoroacetic acid / dichloromethane
8: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane
With
hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; ammonium hydroxide; diphenyl phosphoryl azide; water; sodium carbonate; benzotriazol-1-ol; 1,2-dichloro-ethane; triethylamine; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; tin(ll) chloride; sodium hydroxide; sodium nitrite;
In
tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; water; acetone; toluene;
6: |Curtius Rearrangement / 8: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2015.04.101
- Guidance literature:
-
Multi-step reaction with 7 steps
1: acetone / Reflux
2: 1,2-dichloro-ethane; benzotriazol-1-ol; ammonium hydroxide / tetrahydrofuran; dichloromethane
3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / Reflux
4: sodium hydroxide; water / methanol; tetrahydrofuran
5: diphenyl phosphoryl azide; triethylamine
6: trifluoroacetic acid / dichloromethane
7: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; ammonium hydroxide; diphenyl phosphoryl azide; water; sodium carbonate; benzotriazol-1-ol; 1,2-dichloro-ethane; triethylamine; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide;
In
tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; water; acetone; toluene;
5: |Curtius Rearrangement / 7: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2015.04.101
